dibenzyl ((4R,13R)-5,12-dioxo-1,2-dithio-6,11-diazacyclopentadecane-4,13-diyl)dicarbamate

Base Information

Chemical Name:dibenzyl ((4R,13R)-5,12-dioxo-1,2-dithio-6,11-diazacyclopentadecane-4,13-diyl)dicarbamate
CAS No.:1385775-77-8
Molecular Formula:C₂₆H₃₂N₄O₆S₂
Molecular Weight:560.695
Hs Code.:

Synonyms:dibenzyl ((4R,13R)-5,12-dioxo-1,2-dithio-6,11-diazacyclopentadecane-4,13-diyl)dicarbamate

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Chemical Property of dibenzyl ((4R,13R)-5,12-dioxo-1,2-dithio-6,11-diazacyclopentadecane-4,13-diyl)dicarbamate

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Technology Process of dibenzyl ((4R,13R)-5,12-dioxo-1,2-dithio-6,11-diazacyclopentadecane-4,13-diyl)dicarbamate

There total 2 articles about dibenzyl ((4R,13R)-5,12-dioxo-1,2-dithio-6,11-diazacyclopentadecane-4,13-diyl)dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 850232-61-0
benzyl N-[(1R)-2-(1H-1,2,3-benzotriazol-1-yl)-2-oxo-1-(sulfanylmethyl)ethyl]carbamate

: 110-60-1
1,4-diaminobutane

: 1385775-77-8
dibenzyl ((4R,13R)-5,12-dioxo-1,2-dithio-6,11-diazacyclopentadecane-4,13-diyl)dicarbamate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃;
DOI:10.1111/j.1747-0285.2011.01303.x

Reference yield:

: 57710-80-2
1-benzyloxycarbonyl-1Hbenzo[d][1.2.3]triazole

: 1385775-77-8
dibenzyl ((4R,13R)-5,12-dioxo-1,2-dithio-6,11-diazacyclopentadecane-4,13-diyl)dicarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / water; acetonitrile / 2 h / 20 °C

2.1: thionyl chloride / tetrahydrofuran / 0.33 h / 25 °C

2.2: 2 h / 0 - 5 °C

3.1: triethylamine / tetrahydrofuran / 20 °C

With thionyl chloride; triethylamine; In tetrahydrofuran; water; acetonitrile;
DOI:10.1111/j.1747-0285.2011.01303.x