(E)-2-(hydroxymethyl)cyclopropyl phenyl sulphide

Base Information

Chemical Name:(E)-2-(hydroxymethyl)cyclopropyl phenyl sulphide
CAS No.:80398-84-1
Molecular Formula:C₁₀H₁₂OS
Molecular Weight:180.271
Hs Code.:

Synonyms:(E)-2-(hydroxymethyl)cyclopropyl phenyl sulphide

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Chemical Property of (E)-2-(hydroxymethyl)cyclopropyl phenyl sulphide

Chemical Property:

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Technology Process of (E)-2-(hydroxymethyl)cyclopropyl phenyl sulphide

There total 8 articles about (E)-2-(hydroxymethyl)cyclopropyl phenyl sulphide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: (E)-ethyl 2-(phenylsulfanyl)cyclopropane-1-carboxylate

: 80398-84-1
(E)-2-(hydroxymethyl)cyclopropyl phenyl sulphide

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 25 ℃; for 3h; Inert atmosphere;
DOI:10.1002/ejoc.201701030

Reference yield: 86.0%

: 63196-76-9,116500-60-8,116500-62-0,144407-72-7
Methyl trans-2-phenylthiocyclopropanecarboxylate

: 80398-84-1
(E)-2-(hydroxymethyl)cyclopropyl phenyl sulphide

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; Heating;
DOI:10.1021/jo00343a034

Reference yield:

: 29193-71-3
methyl 4-(phenylsulfanyl)butanoate

: 80398-84-1
(E)-2-(hydroxymethyl)cyclopropyl phenyl sulphide

Guidance literature:: Multi-step reaction with 3 steps

1: N-chlorocuccinimide / CCl₄ / Heating

2: (Me)3COK / tetrahydrofuran / -20 deg C up to r.t.

3: LAH / diethyl ether / Heating

With N-chloro-succinimide; lithium aluminium tetrahydride; potassium tert-butylate; In tetrahydrofuran; tetrachloromethane; diethyl ether;