Technology Process of N-allyl-N-(2-iodoethyl)-2-bromobenzenesulfonamide
There total 3 articles about N-allyl-N-(2-iodoethyl)-2-bromobenzenesulfonamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium iodide;
In
acetone;
at 60 ℃;
for 4h;
Inert atmosphere;
DOI:10.1002/anie.201105235
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 0 - 20 °C
2: sodium iodide / acetone / 4 h / 60 °C / Inert atmosphere
With
triethylamine; sodium iodide;
In
dichloromethane; acetone;
DOI:10.1002/anie.201105235
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere
2: triethylamine / dichloromethane / 0 - 20 °C
3: sodium iodide / acetone / 4 h / 60 °C / Inert atmosphere
With
lithium aluminium tetrahydride; triethylamine; sodium iodide;
In
tetrahydrofuran; dichloromethane; acetone;
DOI:10.1002/anie.201105235
