Ru(OS(CH₃)2)3(CH₃C(CH₂As(C₆H₅)2)3)⁽²⁺⁾*2CF₃SO₃^(1-)={Ru(OS(CH₃)2)3(CH₃C(CH₂As(C₆H₅)2)3)}(CF₃SO₃)2

Base Information

• Chemical Name: Ru(OS(CH₃)2)3(CH₃C(CH₂As(C₆H₅)2)3)⁽²⁺⁾*2CF₃SO₃^(1-)={Ru(OS(CH₃)2)3(CH₃C(CH₂As(C₆H₅)2)3)}(CF₃SO₃)2
• CAS No.: 112220-37-8
• Molecular Formula: 2CF₃O₃S*C₄₇H₅₇As₃O₃RuS₃
• Molecular Weight: 1390.14

Synonyms:Ru(OS(CH₃)2)3(CH₃C(CH₂As(C₆H₅)2)3)⁽²⁺⁾*2CF₃SO₃^(1-)={Ru(OS(CH₃)2)3(CH₃C(CH₂As(C₆H₅)2)3)}(CF₃SO₃)2

Chemical Property of Ru(OS(CH₃)2)3(CH₃C(CH₂As(C₆H₅)2)3)⁽²⁺⁾*2CF₃SO₃^(1-)={Ru(OS(CH₃)2)3(CH₃C(CH₂As(C₆H₅)2)3)}(CF₃SO₃)2

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Technology Process of Ru(OS(CH₃)2)3(CH₃C(CH₂As(C₆H₅)2)3)⁽²⁺⁾*2CF₃SO₃^(1-)={Ru(OS(CH₃)2)3(CH₃C(CH₂As(C₆H₅)2)3)}(CF₃SO₃)2

There total 1 articles about Ru(OS(CH₃)2)3(CH₃C(CH₂As(C₆H₅)2)3)⁽²⁺⁾*2CF₃SO₃^(1-)={Ru(OS(CH₃)2)3(CH₃C(CH₂As(C₆H₅)2)3)}(CF₃SO₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

{Ru(μ-Cl)3(triars)2}Cl (112220-33-4) + silver trifluoromethanesulfonate (2923-28-6) + dimethyl sulfoxide (67-68-5,8070-53-9) → Ru(OS(CH3)2)3(CH3C(CH2As(C6H5)2)3)(2+)*2CF3SO3(1-)={Ru(OS(CH3)2)3(CH3C(CH2As(C6H5)2)3)}(CF3SO3)2 (112220-37-8)

Guidance literature:

In dimethyl sulfoxide; byproducts: AgCl; Ar atmosphere, heating (110°C, 2 h); filtration (Celite, AgCl removal), vol. redn., pptn. (toluene addn.), washing (toluene, Et2O), drying; elem. anal. (1/3 mol toluene solvate found);

Reference yield: 87.0%

Ru(OS(CH3)2)3(CH3C(CH2As(C6H5)2)3)(2+)*2CF3SO3(1-)={Ru(OS(CH3)2)3(CH3C(CH2As(C6H5)2)3)}(CF3SO3)2 (112220-37-8) → Ru(CF3SO3)(CO)2(CH3C(CH2As(C6H5)2)3)(1+)*CF3SO3(1-)={Ru(CF3SO3)(CO)2(CH3C(CH2As(C6H5)2)3)}(CF3SO3) (112220-46-9) + dimethyl sulfoxide (67-68-5,8070-53-9)

Guidance literature:

With CO; In dichloromethane; stirring of soln. under CO atmosphere (3 h); pptn. (Et2O addn.), washing (Et2O), drying; elem. anal.;

upstream raw materials:

{Ru(μ-Cl)3(triars)2}Cl

silver trifluoromethanesulfonate

dimethyl sulfoxide

Downstream raw materials:

Ru(CF₃SO₃)(CO)2(CH₃C(CH₂As(C₆H₅)2)3)⁽¹⁺⁾*CF₃SO₃^(1-)={Ru(CF₃SO₃)(CO)2(CH₃C(CH₂As(C₆H₅)2)3)}(CF₃SO₃)

dimethyl sulfoxide

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