C₅₄H₆₅F₃N₄O₁₁Si

Base Information

Chemical Name:C₅₄H₆₅F₃N₄O₁₁Si
CAS No.:1359025-30-1
Molecular Formula:C₅₄H₆₅F₃N₄O₁₁Si
Molecular Weight:1031.21
Hs Code.:

C<sub>54</sub>H<sub>65</sub>F<sub>3</sub>N<sub>4</sub>O<sub>11</sub>Si

Synonyms:C₅₄H₆₅F₃N₄O₁₁Si

Suppliers and Price of C₅₄H₆₅F₃N₄O₁₁Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₄H₆₅F₃N₄O₁₁Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₄H₆₅F₃N₄O₁₁Si

There total 17 articles about C₅₄H₆₅F₃N₄O₁₁Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4530-20-5
BOC-glycine

: 1359025-19-6
C₄₇H₅₄F₃N₃O₈Si

: 1359025-30-1
C₅₄H₆₅F₃N₄O₁₁Si

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; at 20 ℃;

Reference yield:

: 710-18-9
1-methoxy-4-(trifluoromethoxy)benzene

: 1359025-30-1
C₅₄H₆₅F₃N₄O₁₁Si

Guidance literature:: Multi-step reaction with 17 steps

1.1: sulfuric acid; nitric acid / dichloromethane / 0 - 20 °C

2.1: sodium dithionite; water / tetrahydrofuran / 16 h / 20 °C

3.1: pyridinium hydrobromide perbromide / dichloromethane / 1 h / 0 °C

4.1: hydrogenchloride; sodium nitrite / 1,4-dioxane; water / 0.5 h / 20 °C

4.2: 72 h / 0 - 20 °C

5.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / 1 h / -78 °C

5.2: 2 h / -78 - 20 °C

6.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1.5 h / 0 - 20 °C

7.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 20 °C

8.1: n-butyllithium; Di-sec-butylamin; N,N,N,N,-tetramethylethylenediamine; triethylamine hydrochloride / tetrahydrofuran; hexane / 1 h / -78 °C

8.2: 2.02 h / -78 - 20 °C

9.1: boron tribromide / dichloromethane / 1 h / -78 - 0 °C

9.2: 0.25 h / 20 °C

10.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

11.1: n-butyllithium / tetrahydrofuran / 0.33 h / -100 °C / Inert atmosphere

11.2: 1.08 h / -100 - -78 °C

12.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

13.1: sodium tetrahydroborate / 1,2-dichloro-ethane / 2 h / 20 °C

14.1: potassium carbonate / acetonitrile / 2 h / 30 °C

15.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine; diisopropylamine / tetrahydrofuran; hexane / 0.17 h / -78 °C

15.2: 1 h / -78 - 0 °C

16.1: 1,3-dimethylbarbituric acid / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 24 h / 35 °C / Inert atmosphere

17.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / 20 °C

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; sodium dithionite; oxalyl dichloride; 1,3-dimethylbarbituric acid; Di-sec-butylamin; N,N,N,N,-tetramethylethylenediamine; sulfuric acid; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; isopropylmagnesium chloride; nitric acid; boron tribromide; triethylamine hydrochloride; potassium carbonate; pyridinium hydrobromide perbromide; diisopropylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium chloride; sodium nitrite; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 660848-54-4
1-methoxy-2-nitro-4-(trifluoromethoxy)benzene

: 1359025-30-1
C₅₄H₆₅F₃N₄O₁₁Si

Guidance literature:: Multi-step reaction with 16 steps

1.1: sodium dithionite; water / tetrahydrofuran / 16 h / 20 °C

2.1: pyridinium hydrobromide perbromide / dichloromethane / 1 h / 0 °C

3.1: hydrogenchloride; sodium nitrite / 1,4-dioxane; water / 0.5 h / 20 °C

3.2: 72 h / 0 - 20 °C

4.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / 1 h / -78 °C

4.2: 2 h / -78 - 20 °C

5.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1.5 h / 0 - 20 °C

6.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 20 °C

7.1: n-butyllithium; Di-sec-butylamin; N,N,N,N,-tetramethylethylenediamine; triethylamine hydrochloride / tetrahydrofuran; hexane / 1 h / -78 °C

7.2: 2.02 h / -78 - 20 °C

8.1: boron tribromide / dichloromethane / 1 h / -78 - 0 °C

8.2: 0.25 h / 20 °C

9.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

10.1: n-butyllithium / tetrahydrofuran / 0.33 h / -100 °C / Inert atmosphere

10.2: 1.08 h / -100 - -78 °C

11.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

12.1: sodium tetrahydroborate / 1,2-dichloro-ethane / 2 h / 20 °C

13.1: potassium carbonate / acetonitrile / 2 h / 30 °C

14.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine; diisopropylamine / tetrahydrofuran; hexane / 0.17 h / -78 °C

14.2: 1 h / -78 - 0 °C

15.1: 1,3-dimethylbarbituric acid / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 24 h / 35 °C / Inert atmosphere

16.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / 20 °C

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; sodium dithionite; oxalyl dichloride; 1,3-dimethylbarbituric acid; Di-sec-butylamin; N,N,N,N,-tetramethylethylenediamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; isopropylmagnesium chloride; boron tribromide; triethylamine hydrochloride; potassium carbonate; pyridinium hydrobromide perbromide; diisopropylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium chloride; sodium nitrite; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;