C₁₇H₁₄BrNO₄

Base Information

Chemical Name:C₁₇H₁₄BrNO₄
CAS No.:1355558-32-5
Molecular Formula:C₁₇H₁₄BrNO₄
Molecular Weight:376.206
Hs Code.:

C<sub>17</sub>H<sub>14</sub>BrNO<sub>4</sub>

Synonyms:C₁₇H₁₄BrNO₄

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Chemical Property of C₁₇H₁₄BrNO₄

Chemical Property:

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Technology Process of C₁₇H₁₄BrNO₄

There total 5 articles about C₁₇H₁₄BrNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1355558-58-5
C₂₃H₂₈BrNO₄Si

: 1355558-32-5
C₁₇H₁₄BrNO₄

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1016/j.bmcl.2011.10.095

Reference yield:

: 142613-09-0
N-(4-methoxyphenyl)-N-(prop-2-ynyl)-carbamic acid tert-butyl ester

: 1355558-32-5
C₁₇H₁₄BrNO₄

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; palladium diacetate; triethylamine; triphenylphosphine / toluene / 5 h / 20 °C

2: (triphenylphosphine)gold(I) chloride; silver hexafluoroantimonate / dichloromethane / 1.5 h / 20 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

With silver hexafluoroantimonate; copper(l) iodide; (triphenylphosphine)gold(I) chloride; tetrabutyl ammonium fluoride; palladium diacetate; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; toluene; 1: Sonogashira coupling;
DOI:10.1016/j.bmcl.2011.10.095

Reference yield:

: 18437-68-8
tert-butyl N-(4-methoxyphenyl)carbamate

: 1355558-32-5
C₁₇H₁₄BrNO₄

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C

2: copper(l) iodide; palladium diacetate; triethylamine; triphenylphosphine / toluene / 5 h / 20 °C

3: (triphenylphosphine)gold(I) chloride; silver hexafluoroantimonate / dichloromethane / 1.5 h / 20 °C

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

With silver hexafluoroantimonate; copper(l) iodide; (triphenylphosphine)gold(I) chloride; tetrabutyl ammonium fluoride; palladium diacetate; sodium hydride; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; 2: Sonogashira coupling;
DOI:10.1016/j.bmcl.2011.10.095