allyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-2-O-benzoyl-3-O-chloroacetyl-α-L-rhamnopyranoside

Base Information

Chemical Name:allyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-2-O-benzoyl-3-O-chloroacetyl-α-L-rhamnopyranoside
CAS No.:686767-41-9
Molecular Formula:C₅₂H₅₅ClO₁₂
Molecular Weight:907.454
Hs Code.:

Synonyms:allyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-2-O-benzoyl-3-O-chloroacetyl-α-L-rhamnopyranoside

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Chemical Property of allyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-2-O-benzoyl-3-O-chloroacetyl-α-L-rhamnopyranoside

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Technology Process of allyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-2-O-benzoyl-3-O-chloroacetyl-α-L-rhamnopyranoside

There total 1 articles about allyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-2-O-benzoyl-3-O-chloroacetyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 541-88-8
Chloroacetic anhydride

: 497182-23-7
allyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-4)-2-O-benzoyl-α-L-rhamnopyranoside

: 686767-41-9
allyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-2-O-benzoyl-3-O-chloroacetyl-α-L-rhamnopyranoside

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1016/j.tet.2004.01.054

Reference yield: 97.0%

: 686767-41-9
allyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-2-O-benzoyl-3-O-chloroacetyl-α-L-rhamnopyranoside

: (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-2-O-benzoyl-3-O-chloroacetyl-α/β-L-rhamnopyranose

Guidance literature:: allyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-2-O-benzoyl-3-O-chloroacetyl-α-L-rhamnopyranoside; With (1,5-cyclooctadiene)bis(methyldiphenylphosphine) iridium hexafluorophosphate; In tetrahydrofuran; at 20 ℃; for 3h;

With iodine; In tetrahydrofuran; water; at 20 ℃; for 0.5h; Further stages.;
DOI:10.1016/j.tet.2004.01.054