Methyl 3-(3-Methoxy-4-methylphenyl)-2-methoxycarbonylbutanoate

Base Information

Chemical Name:Methyl 3-(3-Methoxy-4-methylphenyl)-2-methoxycarbonylbutanoate
CAS No.:130921-07-2
Molecular Formula:C₁₅H₂₀O₅
Molecular Weight:280.321
Hs Code.:

Synonyms:Methyl 3-(3-Methoxy-4-methylphenyl)-2-methoxycarbonylbutanoate

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Chemical Property of Methyl 3-(3-Methoxy-4-methylphenyl)-2-methoxycarbonylbutanoate

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Technology Process of Methyl 3-(3-Methoxy-4-methylphenyl)-2-methoxycarbonylbutanoate

There total 5 articles about Methyl 3-(3-Methoxy-4-methylphenyl)-2-methoxycarbonylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3556-83-0
methyl 4-methyl-3-methoxybenzoate

: 130921-07-2
Methyl 3-(3-Methoxy-4-methylphenyl)-2-methoxycarbonylbutanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / LiAlH₄ / diethyl ether / 2.5 h / Heating

2: 90 percent / active MnO₂ / CH₂Cl₂ / 2 h / Heating

3: 91 percent / benzoic acid, piperidine / benzene / Heating

4: 1) CuI / 1) ether, -78 deg C, 30 min, 2) -78 deg C, 2h, to room temp.

With piperidine; manganese(IV) oxide; copper(l) iodide; lithium aluminium tetrahydride; benzoic acid; In diethyl ether; dichloromethane; benzene;
DOI:10.1248/cpb.38.1852

Reference yield:

: 7151-68-0
3-methoxy-p-toluic acid

: 130921-07-2
Methyl 3-(3-Methoxy-4-methylphenyl)-2-methoxycarbonylbutanoate

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / acetic acid / diethyl ether

2: 88 percent / LiAlH₄ / diethyl ether / 2.5 h / Heating

3: 90 percent / active MnO₂ / CH₂Cl₂ / 2 h / Heating

4: 91 percent / benzoic acid, piperidine / benzene / Heating

5: 1) CuI / 1) ether, -78 deg C, 30 min, 2) -78 deg C, 2h, to room temp.

With piperidine; manganese(IV) oxide; copper(l) iodide; lithium aluminium tetrahydride; acetic acid; benzoic acid; In diethyl ether; dichloromethane; benzene;
DOI:10.1248/cpb.38.1852

Reference yield:

: 4685-50-1
3-methoxy-4-methylbenzyl alcohol

: 130921-07-2
Methyl 3-(3-Methoxy-4-methylphenyl)-2-methoxycarbonylbutanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / active MnO₂ / CH₂Cl₂ / 2 h / Heating

2: 91 percent / benzoic acid, piperidine / benzene / Heating

3: 1) CuI / 1) ether, -78 deg C, 30 min, 2) -78 deg C, 2h, to room temp.

With piperidine; manganese(IV) oxide; copper(l) iodide; benzoic acid; In dichloromethane; benzene;
DOI:10.1248/cpb.38.1852