3-(3-methoxy-4-methyl-phenyl)-butyric acid

Base Information

Chemical Name:3-(3-methoxy-4-methyl-phenyl)-butyric acid
CAS No.:34638-69-2
Molecular Formula:C₁₂H₁₆O₃
Molecular Weight:208.257
Hs Code.:

Synonyms:3-(3-methoxy-4-methyl-phenyl)-butyric acid

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Chemical Property of 3-(3-methoxy-4-methyl-phenyl)-butyric acid

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Technology Process of 3-(3-methoxy-4-methyl-phenyl)-butyric acid

There total 9 articles about 3-(3-methoxy-4-methyl-phenyl)-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3556-83-0
methyl 4-methyl-3-methoxybenzoate

: 34638-69-2
3-(3-methoxy-4-methyl-phenyl)-butyric acid

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / LiAlH₄ / diethyl ether / 2.5 h / Heating

2: 90 percent / active MnO₂ / CH₂Cl₂ / 2 h / Heating

3: 91 percent / benzoic acid, piperidine / benzene / Heating

4: 1) CuI / 1) ether, -78 deg C, 30 min, 2) -78 deg C, 2h, to room temp.

5: 1) KOH / 1) aq. EtOH, 2) 150 - 170 deg C

With piperidine; manganese(IV) oxide; potassium hydroxide; copper(l) iodide; lithium aluminium tetrahydride; benzoic acid; In diethyl ether; dichloromethane; benzene;
DOI:10.1248/cpb.38.1852

Reference yield:

: 7151-68-0
3-methoxy-p-toluic acid

: 34638-69-2
3-(3-methoxy-4-methyl-phenyl)-butyric acid

Guidance literature:: Multi-step reaction with 6 steps

1: 91 percent / acetic acid / diethyl ether

2: 88 percent / LiAlH₄ / diethyl ether / 2.5 h / Heating

3: 90 percent / active MnO₂ / CH₂Cl₂ / 2 h / Heating

4: 91 percent / benzoic acid, piperidine / benzene / Heating

5: 1) CuI / 1) ether, -78 deg C, 30 min, 2) -78 deg C, 2h, to room temp.

6: 1) KOH / 1) aq. EtOH, 2) 150 - 170 deg C

With piperidine; manganese(IV) oxide; potassium hydroxide; copper(l) iodide; lithium aluminium tetrahydride; acetic acid; benzoic acid; In diethyl ether; dichloromethane; benzene;
DOI:10.1248/cpb.38.1852

Reference yield:

: 24973-22-6
3-methoxy-4-methylbenzaldehyde

: 34638-69-2
3-(3-methoxy-4-methyl-phenyl)-butyric acid

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / benzoic acid, piperidine / benzene / Heating

2: 1) CuI / 1) ether, -78 deg C, 30 min, 2) -78 deg C, 2h, to room temp.

3: 1) KOH / 1) aq. EtOH, 2) 150 - 170 deg C

With piperidine; potassium hydroxide; copper(l) iodide; benzoic acid; In benzene;
DOI:10.1248/cpb.38.1852