(-)-(2R,3S,6'R,1''S)-3-Methyl-N-<6'-(2''-nitro-1''-phenylaethyl)-1-cyclohexenyl>-2-phenylmorpholin

Base Information

Chemical Name:(-)-(2R,3S,6'R,1''S)-3-Methyl-N-<6'-(2''-nitro-1''-phenylaethyl)-1-cyclohexenyl>-2-phenylmorpholin
CAS No.:83976-49-2
Molecular Formula:C₂₅H₃₀N₂O₃
Molecular Weight:406.525
Hs Code.:

Synonyms:(-)-(2R,3S,6'R,1''S)-3-Methyl-N-<6'-(2''-nitro-1''-phenylaethyl)-1-cyclohexenyl>-2-phenylmorpholin

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Chemical Property of (-)-(2R,3S,6'R,1''S)-3-Methyl-N-<6'-(2''-nitro-1''-phenylaethyl)-1-cyclohexenyl>-2-phenylmorpholin

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Technology Process of (-)-(2R,3S,6'R,1''S)-3-Methyl-N-<6'-(2''-nitro-1''-phenylaethyl)-1-cyclohexenyl>-2-phenylmorpholin

There total 3 articles about (-)-(2R,3S,6'R,1''S)-3-Methyl-N-<6'-(2''-nitro-1''-phenylaethyl)-1-cyclohexenyl>-2-phenylmorpholin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 5153-67-3
nitrostyrene

: 83976-43-6
(2R,3S)-N-(1'-Cyclohexenyl)-3-methyl-2-phenylmorpholin

: 83976-49-2
(-)-(2R,3S,6'R,1''S)-3-Methyl-N-<6'-(2''-nitro-1''-phenylaethyl)-1-cyclohexenyl>-2-phenylmorpholin

: 84025-88-7
(+)-(2R,3S,6'S,1''R)-3-Methyl-N-<6'-(2''-nitro-1''-phenylaethyl)-1-cyclohexenyl>-2-phenylmorpholin

Guidance literature:: In diethyl ether; for 72h; Ambient temperature;
DOI:10.1002/hlca.19820650537

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 83976-49-2
(-)-(2R,3S,6'R,1''S)-3-Methyl-N-<6'-(2''-nitro-1''-phenylaethyl)-1-cyclohexenyl>-2-phenylmorpholin

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / p-toluenesulfonic acid / benzene / 22 h / Heating

2: 23 percent / diethyl ether / 72 h / Ambient temperature

With toluene-4-sulfonic acid; In diethyl ether; benzene;
DOI:10.1002/hlca.19820650537

Reference yield:

: 84025-82-1,21288-73-3
(-)-(2R,3S)-3-Methyl-2-phenylmorpholin

: 83976-49-2
(-)-(2R,3S,6'R,1''S)-3-Methyl-N-<6'-(2''-nitro-1''-phenylaethyl)-1-cyclohexenyl>-2-phenylmorpholin

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / p-toluenesulfonic acid / benzene / 22 h / Heating

2: 23 percent / diethyl ether / 72 h / Ambient temperature

With toluene-4-sulfonic acid; In diethyl ether; benzene;
DOI:10.1002/hlca.19820650537