Boc-Leu-NHC₆H₄COOEt

Base Information

• Chemical Name: Boc-Leu-NHC₆H₄COOEt
• CAS No.: 59190-90-8
• Molecular Formula: C₂₀H₃₀N₂O₅
• Molecular Weight: 378.469

Synonyms:Boc-Leu-NHC₆H₄COOEt

Chemical Property of Boc-Leu-NHC₆H₄COOEt

Chemical Property:

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Technology Process of Boc-Leu-NHC₆H₄COOEt

There total 1 articles about Boc-Leu-NHC₆H₄COOEt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

N-tert-butoxycarbonyl-L-leucine (13139-15-6,53296-34-7) + p-aminoethylbenzoate (94-09-7) → Boc-Leu-NHC6H4COOEt (59190-90-8)

Guidance literature:

With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;

DOI:10.1021/ja044310j

Reference yield: 86.0%

Boc-Leu-NHC6H4COOEt (59190-90-8) → 4-((S)-2-Amino-4-methyl-pentanoylamino)-benzoic acid ethyl ester; hydrochloride

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 20 ℃;

DOI:10.1021/ja044310j

Reference yield: 73.0%

Boc-Leu-NHC6H4COOEt (59190-90-8) → 4-(2-tert-butoxycarbonylamino-4-methyl-pentanoylamino)-benzoic acid (823786-66-9)

Guidance literature:

With sodium hydroxide; In ethanol; at 20 ℃; for 24h;

DOI:10.1021/ja044310j

upstream raw materials:

N-tert-butoxycarbonyl-L-leucine

p-aminoethylbenzoate

Downstream raw materials:

4-(2-tert-butoxycarbonylamino-4-methyl-pentanoylamino)-benzoic acid

[1-(4-tert-butylcarbamoyl-phenylcarbamoyl)-3-methyl-butyl]-carbamic acid tert-butyl ester

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