Thiocarbonic acid O-((S)-2-benzyloxy-1-iodomethyl-ethyl) ester S-methyl ester

Base Information

Chemical Name:Thiocarbonic acid O-((S)-2-benzyloxy-1-iodomethyl-ethyl) ester S-methyl ester
CAS No.:172657-91-9
Molecular Formula:C₁₂H₁₅IO₃S
Molecular Weight:366.22
Hs Code.:

Synonyms:Thiocarbonic acid O-((S)-2-benzyloxy-1-iodomethyl-ethyl) ester S-methyl ester

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Chemical Property of Thiocarbonic acid O-((S)-2-benzyloxy-1-iodomethyl-ethyl) ester S-methyl ester

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Technology Process of Thiocarbonic acid O-((S)-2-benzyloxy-1-iodomethyl-ethyl) ester S-methyl ester

There total 2 articles about Thiocarbonic acid O-((S)-2-benzyloxy-1-iodomethyl-ethyl) ester S-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 172657-90-8
(S)-4-Benzyloxymethyl-[1,3]dioxolane-2-thione

: 74-88-4
methyl iodide

: 172657-91-9
Thiocarbonic acid O-((S)-2-benzyloxy-1-iodomethyl-ethyl) ester S-methyl ester

Guidance literature:: In 1,2-dichloro-ethane; for 18h; Heating;
DOI:10.1016/0040-4039(95)01658-9

Reference yield:

: 56552-80-8
(R)-3-benzyloxy-1,2-propanediol

: 172657-91-9
Thiocarbonic acid O-((S)-2-benzyloxy-1-iodomethyl-ethyl) ester S-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / 1,2-dichloro-ethane / 18 h / Ambient temperature

2: 96 percent / 1,2-dichloro-ethane / 18 h / Heating

In 1,2-dichloro-ethane;
DOI:10.1016/0040-4039(95)01658-9