4,4'-dimethoxybenzhydryl ethyl ether

Base Information

• Chemical Name: 4,4'-dimethoxybenzhydryl ethyl ether
• CAS No.: 74684-95-0
• Molecular Formula: C₁₇H₂₀O₃
• Molecular Weight: 272.344
• Mol file: 74684-95-0.mol

Synonyms:4,4'-dimethoxybenzhydryl ethyl ether

Chemical Property of 4,4'-dimethoxybenzhydryl ethyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,4'-dimethoxybenzhydryl ethyl ether

There total 16 articles about 4,4'-dimethoxybenzhydryl ethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

ethanol (64-17-5) + 4,4'-Dimethoxybenzhydrol (728-87-0) → 4,4'-dimethoxybenzhydryl ethyl ether (74684-95-0)

Guidance literature:

With copper(ll) bromide; at 20 ℃; for 1.5h;

DOI:10.1016/j.tetlet.2009.10.053

Reference yield: 60.0%

ethanol (64-17-5) + Bis(p-methoxyphenyl)diazomethan (1221-72-3) → 4,4'-dimethoxybenzhydryl ethyl ether (74684-95-0)

Guidance literature:

for 1.5h; Reflux;

DOI:10.1016/j.tetlet.2011.01.116

Reference yield:

ethanol (64-17-5) + bis(4-methoxyphenyl)methyl 4-cyanophenyl ether (116664-86-9) → 4,4'-dimethoxybenzhydryl ethyl ether (74684-95-0) + 4,4'-Dimethoxybenzhydrol (728-87-0)

Guidance literature:

With water; at 20 ℃; Kinetics; Flash photolysis;

DOI:10.1021/ja031828z

upstream raw materials:

4,4'-dimethoxydiphenylmethyl chloride

bis-(4-methoxy-phenyl)-(toluene-4-sulfonyl)-methane

ethanol

bis(4-methoxyphenyl)thione