cis-N,N'-bis-allyl-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

Base Information

Chemical Name:cis-N,N'-bis-allyl-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene
CAS No.:934389-55-6
Molecular Formula:C₂₆H₃₂N₂O₄S₂
Molecular Weight:500.683
Hs Code.:

Synonyms:cis-N,N'-bis-allyl-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

Suppliers and Price of cis-N,N'-bis-allyl-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of cis-N,N'-bis-allyl-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of cis-N,N'-bis-allyl-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

There total 4 articles about cis-N,N'-bis-allyl-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 934389-54-5
cis-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

: 106-95-6
allyl bromide

: 934389-55-6
cis-N,N'-bis-allyl-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.01.092

Reference yield: 43.0%

: 934389-54-5
cis-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

: 106-95-6
allyl bromide

: cis-N-allyl-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

: 934389-55-6
cis-N,N'-bis-allyl-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

Guidance literature:: cis-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 2h;

allyl bromide; In N,N-dimethyl-formamide; at 0 - 20 ℃; Further stages.;
DOI:10.1016/j.tet.2007.10.076

Reference yield:

: 102312-67-4,105249-35-2,108796-57-2,118157-55-4
cis-cyclohex-3-enyl-1,2-diamine dihydrochloride

: 934389-55-6
cis-N,N'-bis-allyl-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / Et₃N / CH₂Cl₂

2: 98 percent / NaH / dimethylformamide

With sodium hydride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.01.092