benzyl 3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl>-β-D-erythro-hept-5-enofuranuronate

Base Information

Chemical Name:benzyl 3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl>-β-D-erythro-hept-5-enofuranuronate
CAS No.:75863-42-2
Molecular Formula:C₂₈H₂₈N₂O₇
Molecular Weight:504.54
Hs Code.:

Synonyms:benzyl 3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl>-β-D-erythro-hept-5-enofuranuronate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl>-β-D-erythro-hept-5-enofuranuronate

Chemical Property:

Purity/Quality:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of benzyl 3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl>-β-D-erythro-hept-5-enofuranuronate

There total 6 articles about benzyl 3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl>-β-D-erythro-hept-5-enofuranuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21090-30-2
3'-O-acetylthymidine

: 75863-42-2
benzyl 3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl>-β-D-erythro-hept-5-enofuranuronate

Guidance literature:: Multi-step reaction with 4 steps

2: Dowex 5OW-X₈(H(+)) / H₂O; tetrahydrofuran / 6 h

3: 54 percent / acetonitrile / 20 h / Ambient temperature

4: pyridine / 1) 1h, cold, 2) 40h at ambient temp.

With Dowex 5OW-X₈(H(+)); In tetrahydrofuran; pyridine; water; acetonitrile;
DOI:10.1021/jo00316a021

Reference yield:

: 75863-39-7
Acetic acid (2R,3S,5R)-2-(1,3-diphenyl-imidazolidin-2-yl)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

: 75863-42-2
benzyl 3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl>-β-D-erythro-hept-5-enofuranuronate

Guidance literature:: Multi-step reaction with 3 steps

1: Dowex 5OW-X₈(H(+)) / H₂O; tetrahydrofuran / 6 h

2: 54 percent / acetonitrile / 20 h / Ambient temperature

3: pyridine / 1) 1h, cold, 2) 40h at ambient temp.

With Dowex 5OW-X₈(H(+)); In tetrahydrofuran; pyridine; water; acetonitrile;
DOI:10.1021/jo00316a021

Reference yield:

: 15097-38-8
(carbobenzyloxymethylene)triphenylphosphorane

: 75863-42-2
benzyl 3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl>-β-D-erythro-hept-5-enofuranuronate

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / acetonitrile / 20 h / Ambient temperature

2: pyridine / 1) 1h, cold, 2) 40h at ambient temp.

In pyridine; acetonitrile;
DOI:10.1021/jo00316a021