C₃₃H₃₄N₂O₉

Base Information

Chemical Name:C₃₃H₃₄N₂O₉
CAS No.:1446748-47-5
Molecular Formula:C₃₃H₃₄N₂O₉
Molecular Weight:602.641
Hs Code.:

C<sub>33</sub>H<sub>34</sub>N<sub>2</sub>O<sub>9</sub>

Synonyms:C₃₃H₃₄N₂O₉

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Chemical Property of C₃₃H₃₄N₂O₉

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Technology Process of C₃₃H₃₄N₂O₉

There total 10 articles about C₃₃H₃₄N₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1446748-46-4
2'-O,4'-C-ethyleneoxy-5-methyluridine

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1446748-47-5
C₃₃H₃₄N₂O₉

Guidance literature:: With pyridine; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol401566r

Reference yield:

: 1446748-41-9
C₃₃H₄₆N₂O₉Si

: 1446748-47-5
C₃₃H₃₄N₂O₉

Guidance literature:: Multi-step reaction with 6 steps

1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

3: pyridine / 1 h / 0 °C / Inert atmosphere

4: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

5: 20% palladium hydroxide-activated charcoal; cyclohexene / ethanol / Reflux; Inert atmosphere

6: pyridine / 0 - 20 °C / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; 20% palladium hydroxide-activated charcoal; tetrabutyl ammonium fluoride; sodium hydride; cyclohexene; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol401566r

Reference yield:

: 1446748-43-1
C₄₈H₅₀N₂O₁₁

: 1446748-47-5
C₃₃H₃₄N₂O₉

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 1 h / 0 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

3: 20% palladium hydroxide-activated charcoal; cyclohexene / ethanol / Reflux; Inert atmosphere

4: pyridine / 0 - 20 °C / Inert atmosphere

With pyridine; 20% palladium hydroxide-activated charcoal; sodium hydride; cyclohexene; In ethanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol401566r