N-(1,1,2-trimethyl-2-propenylpentafluorophenyl)hydroxylamine

Base Information

• Chemical Name: N-(1,1,2-trimethyl-2-propenylpentafluorophenyl)hydroxylamine
• CAS No.: 30287-20-8
• Molecular Formula: C₁₂H₁₂F₅NO
• Molecular Weight: 281.225
• Mol file: 30287-20-8.mol

Synonyms:N-(1,1,2-trimethyl-2-propenylpentafluorophenyl)hydroxylamine

Chemical Property of N-(1,1,2-trimethyl-2-propenylpentafluorophenyl)hydroxylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(1,1,2-trimethyl-2-propenylpentafluorophenyl)hydroxylamine

There total 3 articles about N-(1,1,2-trimethyl-2-propenylpentafluorophenyl)hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-Dimethyl-2-butene (563-79-1) + pentafluoronitrosobenzene (1423-13-8) + 1,1,1,4,4,4-hexadeuterio-2,3-bis(trideuteriomethyl)but-2-ene (69165-86-2) → N-(1,1,2-trimethyl-2-propenylpentafluorophenyl)hydroxylamine (30287-20-8) + C12(2)H12F5NO

Guidance literature:

In dichloromethane; at 0 ℃; for 0.5h; Further Variations:; Solvents; Kinetics;

DOI:10.1021/jo0266240

Reference yield:

2,3-Dimethyl-2-butene (563-79-1) + pentafluoronitrosobenzene (1423-13-8) → N-(1,1,2-trimethyl-2-propenylpentafluorophenyl)hydroxylamine (30287-20-8)

Guidance literature:

Mechanism; isotope effect;

DOI:10.1021/jo00147a044

Reference yield:

→ N-(1,1,2-trimethyl-2-propenylpentafluorophenyl)hydroxylamine (30287-20-8)

Guidance literature:

Pentafluornitrosobenzol, Triethylphosphit, Tetramethylethylen;

DOI:10.1039/c39720001160

upstream raw materials:

2,3-Dimethyl-2-butene

pentafluoronitrosobenzene

1,1,1,4,4,4-hexadeuterio-2,3-bis(trideuteriomethyl)but-2-ene

Downstream raw materials:

N-Pentafluorophenyl-N-(1,1,2-trimethyl-propyl)-hydroxylamine