(1E,3Z)-4-{o-[(1E,3Z)-3-chloro-4-phenyl-1,3-butadienyl]phenyl}-2-chloro-1-phenyl-1,3-butadiene

Base Information

• Chemical Name: (1E,3Z)-4-{o-[(1E,3Z)-3-chloro-4-phenyl-1,3-butadienyl]phenyl}-2-chloro-1-phenyl-1,3-butadiene
• CAS No.: 1463930-92-8
• Molecular Formula: C₂₆H₂₀Cl₂
• Molecular Weight: 403.351

Synonyms:(1E,3Z)-4-{o-[(1E,3Z)-3-chloro-4-phenyl-1,3-butadienyl]phenyl}-2-chloro-1-phenyl-1,3-butadiene

Chemical Property of (1E,3Z)-4-{o-[(1E,3Z)-3-chloro-4-phenyl-1,3-butadienyl]phenyl}-2-chloro-1-phenyl-1,3-butadiene

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Technology Process of (1E,3Z)-4-{o-[(1E,3Z)-3-chloro-4-phenyl-1,3-butadienyl]phenyl}-2-chloro-1-phenyl-1,3-butadiene

There total 3 articles about (1E,3Z)-4-{o-[(1E,3Z)-3-chloro-4-phenyl-1,3-butadienyl]phenyl}-2-chloro-1-phenyl-1,3-butadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

(Z)-2-chloro-3-phenyl-2-propenal (33603-89-3) + o-xylylene(bistriphenylphospine) dibromide (1519-46-6) → (1E,3Z)-4-{o-[(1E,3Z)-3-chloro-4-phenyl-1,3-butadienyl]phenyl}-2-chloro-1-phenyl-1,3-butadiene (1463930-92-8)

Guidance literature:

With sodium ethanolate; In ethanol;

DOI:10.1016/j.molstruc.2014.04.028

Reference yield: 6.0%

(Z)-2-chloro-3-phenyl-2-propenal (33603-89-3) + o-xylylene(bistriphenylphospine) dibromide (1519-46-6) → (1Z,3Z)-4-{o-[(1Z,3Z)-3-chloro-4-phenyl-1,3-butadienyl]phenyl}-2-chloro-1-phenyl-1,3-butadiene (1463930-98-4) + C26H20Cl2 (1463931-00-1) + (1E,3Z)-4-{o-[(1E,3Z)-3-chloro-4-phenyl-1,3-butadienyl]phenyl}-2-chloro-1-phenyl-1,3-butadiene (1463930-92-8)

Guidance literature:

With sodium ethanolate; In ethanol; Overall yield = 55 %;

DOI:10.1016/j.molstruc.2013.07.052

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + α-chlorocinnamaldehyde (99414-74-1) + triphenylphosphine (603-35-0) → (1Z,3Z)-4-{o-[(1Z,3Z)-3-chloro-4-phenyl-1,3-butadienyl]phenyl}-2-chloro-1-phenyl-1,3-butadiene (1463930-98-4) + (1E,3Z)-4-{o-[(1E,3Z)-3-chloro-4-phenyl-1,3-butadienyl]phenyl}-2-chloro-1-phenyl-1,3-butadiene (1463930-92-8) + (1E,3E)-4-{o-[(1E,3E)-3-chloro-4-phenyl-1,3-butadienyl]phenyl}-2-chloro-1-phenyl-1,3-butadiene

Guidance literature:

With sodium ethanolate; In ethanol;

DOI:10.1016/j.tet.2013.12.027

upstream raw materials:

(Z)-2-chloro-3-phenyl-2-propenal

o-xylylene(bistriphenylphospine) dibromide

formaldehyd

α-chlorocinnamaldehyde

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