t-butyl 3-benzyl-3-ethoxycarbonylacetyl-2-(ethoxycarbonylmethyl)carbazate

Base Information

Chemical Name:t-butyl 3-benzyl-3-ethoxycarbonylacetyl-2-(ethoxycarbonylmethyl)carbazate
CAS No.:111709-12-7
Molecular Formula:C₂₁H₃₀N₂O₇
Molecular Weight:422.478
Hs Code.:

Synonyms:t-butyl 3-benzyl-3-ethoxycarbonylacetyl-2-(ethoxycarbonylmethyl)carbazate

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Chemical Property of t-butyl 3-benzyl-3-ethoxycarbonylacetyl-2-(ethoxycarbonylmethyl)carbazate

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Technology Process of t-butyl 3-benzyl-3-ethoxycarbonylacetyl-2-(ethoxycarbonylmethyl)carbazate

There total 3 articles about t-butyl 3-benzyl-3-ethoxycarbonylacetyl-2-(ethoxycarbonylmethyl)carbazate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 111709-11-6
t-butyl 3-benzyl-2-(ethoxycarbonylmethyl)carbazate

: 36239-09-5
ethyl chlorocarbonylacetate

: 111709-12-7
t-butyl 3-benzyl-3-ethoxycarbonylacetyl-2-(ethoxycarbonylmethyl)carbazate

Guidance literature:: With triethylamine; In benzene; for 12h; Ambient temperature;

Reference yield:

: 24469-50-9
t-butyl 3-benzylidenecarbazate

: 111709-12-7
t-butyl 3-benzyl-3-ethoxycarbonylacetyl-2-(ethoxycarbonylmethyl)carbazate

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / K₂CO₃ / acetone / 24 h / Heating

2: 95 percent / H₂ / 10 percent Pd-C / ethanol

3: 53 percent / triethylamine / benzene / 12 h / Ambient temperature

With hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In ethanol; acetone; benzene;

Reference yield:

: 111709-10-5
t-butyl 3-benzylidene-2-(ethoxycarbonylmethyl)carbazate

: 111709-12-7
t-butyl 3-benzyl-3-ethoxycarbonylacetyl-2-(ethoxycarbonylmethyl)carbazate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / H₂ / 10 percent Pd-C / ethanol

2: 53 percent / triethylamine / benzene / 12 h / Ambient temperature

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; benzene;