(S)-1,3,5-Tris(1-methoxycarbonylethoxymethylene)-2,4,6-trimethylbenzene

Base Information

• Chemical Name: (S)-1,3,5-Tris(1-methoxycarbonylethoxymethylene)-2,4,6-trimethylbenzene
• CAS No.: 268225-51-0
• Molecular Formula: C₂₄H₃₆O₉
• Molecular Weight: 468.544
• Mol file: 268225-51-0.mol

Synonyms:(S)-1,3,5-Tris(1-methoxycarbonylethoxymethylene)-2,4,6-trimethylbenzene

Chemical Property of (S)-1,3,5-Tris(1-methoxycarbonylethoxymethylene)-2,4,6-trimethylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (S)-1,3,5-Tris(1-methoxycarbonylethoxymethylene)-2,4,6-trimethylbenzene

There total 1 articles about (S)-1,3,5-Tris(1-methoxycarbonylethoxymethylene)-2,4,6-trimethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

(S)-Methyl lactate (27871-49-4,2155-30-8) + 1,3,5-tris(bromomethyl)-2,4,6-trimethylbenzene (21988-87-4) → (S)-1,3,5-Tris(1-methoxycarbonylethoxymethylene)-2,4,6-trimethylbenzene (268225-51-0)

Guidance literature:

(S)-Methyl lactate; With sodium hydride; In tetrahydrofuran; for 0.5h;

1,3,5-tris(bromomethyl)-2,4,6-trimethylbenzene; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; at 20 ℃;

DOI:10.1055/s-2000-6255

Reference yield: 63.0%

methylmagnesium bromide (75-16-1) + (S)-1,3,5-Tris(1-methoxycarbonylethoxymethylene)-2,4,6-trimethylbenzene (268225-51-0) → (S)-1,3,5-Tris(2-hydroxy-2-methylbut-3-oxymethylene)-2,4,6-trimethylbenzene

Guidance literature:

In diethyl ether; for 20h;

DOI:10.1055/s-2000-6255

upstream raw materials:

(S)-Methyl lactate

1,3,5-tris(bromomethyl)-2,4,6-trimethylbenzene