9-(N,N-bis(1H,1H,2H,2H-perfluorooctyl)amino)-N-(2,5-di-tert-butylphenyl)perylene-3,4-dicarboximide

Base Information

Chemical Name:9-(N,N-bis(1H,1H,2H,2H-perfluorooctyl)amino)-N-(2,5-di-tert-butylphenyl)perylene-3,4-dicarboximide
CAS No.:1352541-93-5
Molecular Formula:C₅₂H₃₈F₂₆N₂O₂
Molecular Weight:1216.84
Hs Code.:

Synonyms:9-(N,N-bis(1H,1H,2H,2H-perfluorooctyl)amino)-N-(2,5-di-tert-butylphenyl)perylene-3,4-dicarboximide

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Chemical Property of 9-(N,N-bis(1H,1H,2H,2H-perfluorooctyl)amino)-N-(2,5-di-tert-butylphenyl)perylene-3,4-dicarboximide

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Technology Process of 9-(N,N-bis(1H,1H,2H,2H-perfluorooctyl)amino)-N-(2,5-di-tert-butylphenyl)perylene-3,4-dicarboximide

There total 6 articles about 9-(N,N-bis(1H,1H,2H,2H-perfluorooctyl)amino)-N-(2,5-di-tert-butylphenyl)perylene-3,4-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 67510-50-3
N,N-bis(1H,1H,2H,2H-perfluorooctyl)amine

: 165261-51-8
9-bromo-N-(2,5-di-tert-butylphenyl)-perylene-3,4-dicarboxylic imide

: 1352541-93-5
9-(N,N-bis(1H,1H,2H,2H-perfluorooctyl)amino)-N-(2,5-di-tert-butylphenyl)perylene-3,4-dicarboximide

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate; In toluene; at 90 ℃;
DOI:10.1039/c1gc15864c

Reference yield:

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 1352541-93-5
9-(N,N-bis(1H,1H,2H,2H-perfluorooctyl)amino)-N-(2,5-di-tert-butylphenyl)perylene-3,4-dicarboximide

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole; zinc(II) acetate dihydrate / water / 20 h / 190 °C / Autoclave

2: bromine; potassium carbonate / chlorobenzene / 2.5 h / 40 - 50 °C

3: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate / toluene / 90 °C

With 1H-imidazole; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; bromine; zinc(II) acetate dihydrate; potassium carbonate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate; In water; chlorobenzene; toluene; 3: Hartwig-Buchwald amination;
DOI:10.1039/c1gc15864c

Reference yield:

: 165261-25-6
N-(2,5-di-tert-butylphenyl)-perylene-3,4-dicarboxylic imide

: 1352541-93-5
9-(N,N-bis(1H,1H,2H,2H-perfluorooctyl)amino)-N-(2,5-di-tert-butylphenyl)perylene-3,4-dicarboximide

Guidance literature:: Multi-step reaction with 2 steps

1: bromine; potassium carbonate / chlorobenzene / 2.5 h / 40 - 50 °C

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate / toluene / 90 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; bromine; potassium carbonate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate; In chlorobenzene; toluene; 2: Hartwig-Buchwald amination;
DOI:10.1039/c1gc15864c