6α-Deuteriobenzylpenicillin Benzyl Ester

Base Information

Chemical Name:6α-Deuteriobenzylpenicillin Benzyl Ester
CAS No.:76757-89-6
Molecular Formula:C₂₃H₂₄N₂O₄S
Molecular Weight:425.513
Hs Code.:

Synonyms:6α-Deuteriobenzylpenicillin Benzyl Ester

Suppliers and Price of 6α-Deuteriobenzylpenicillin Benzyl Ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6α-Deuteriobenzylpenicillin Benzyl Ester

Chemical Property:

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Technology Process of 6α-Deuteriobenzylpenicillin Benzyl Ester

There total 2 articles about 6α-Deuteriobenzylpenicillin Benzyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 76757-87-4
6-Deuteriobenzylpenicillin (S)-S-Oxide Benzyl Ester

: 76757-89-6
6α-Deuteriobenzylpenicillin Benzyl Ester

Guidance literature:: With phosphorus tribromide; In N,N-dimethyl-formamide; at -18 ℃; for 0.25h;
DOI:10.1021/jo00323a013

Reference yield:

: 54275-92-2
6-β-phenylacetamidopenicillanic acid-(1S)-oxide

: 76757-89-6
6α-Deuteriobenzylpenicillin Benzyl Ester

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / Et₃N, D₂O / acetonitrile / 24 h / 22 °C

2: 91 percent / PBr₃ / dimethylformamide / 0.25 h / -18 °C

With water-d2; phosphorus tribromide; triethylamine; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo00323a013

Reference yield:

: 76757-89-6
6α-Deuteriobenzylpenicillin Benzyl Ester

: 731751-10-3
6α-Deuteriobenzylpenicillin

Guidance literature:: With hydrogen; potassium hydrogencarbonate; palladium on activated charcoal; In water; acetone; for 3h; under 2574.3 Torr; Ambient temperature;
DOI:10.1021/jo00323a013