Technology Process of C20H20N7O11PS
There total 3 articles about C20H20N7O11PS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ammonium acetate; acetic acid; aniline;
In
water;
at 20 ℃;
for 24h;
pH=4.5;
Inert atmosphere;
DOI:10.1002/cplu.201200056
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; caesium carbonate / water; acetonitrile / 1 h / 100 °C / Inert atmosphere
2: aniline; ammonium acetate; acetic acid / water / 24 h / 20 °C / pH 4.5 / Inert atmosphere
With
ammonium acetate; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; caesium carbonate; acetic acid; aniline;
In
water; acetonitrile;
1: |Suzuki Coupling;
DOI:10.1002/cplu.201200056
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; caesium carbonate / water; acetonitrile / 1 h / 100 °C / Inert atmosphere
2: aniline; ammonium acetate; acetic acid / water / 24 h / 20 °C / pH 4.5 / Inert atmosphere
With
ammonium acetate; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; caesium carbonate; acetic acid; aniline;
In
water; acetonitrile;
1: |Suzuki Coupling;
DOI:10.1002/cplu.201200056