Methanesulfonic acid 1-cyanomethyl-2,6-dimethoxy-cyclohexa-2,5-dienylmethyl ester

Base Information

Chemical Name:Methanesulfonic acid 1-cyanomethyl-2,6-dimethoxy-cyclohexa-2,5-dienylmethyl ester
CAS No.:182363-79-7
Molecular Formula:C₁₂H₁₇NO₅S
Molecular Weight:287.337
Hs Code.:

Synonyms:Methanesulfonic acid 1-cyanomethyl-2,6-dimethoxy-cyclohexa-2,5-dienylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanesulfonic acid 1-cyanomethyl-2,6-dimethoxy-cyclohexa-2,5-dienylmethyl ester

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Technology Process of Methanesulfonic acid 1-cyanomethyl-2,6-dimethoxy-cyclohexa-2,5-dienylmethyl ester

There total 2 articles about Methanesulfonic acid 1-cyanomethyl-2,6-dimethoxy-cyclohexa-2,5-dienylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 124-63-0
methanesulfonyl chloride

: (1-Hydroxymethyl-2,6-dimethoxy-cyclohexa-2,5-dienyl)-acetonitrile

: 182363-79-7
Methanesulfonic acid 1-cyanomethyl-2,6-dimethoxy-cyclohexa-2,5-dienylmethyl ester

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1016/0040-4039(96)01246-4

Reference yield:

: 182363-75-3
1-Cyanomethyl-2,6-dimethoxy-cyclohexa-2,5-dienecarboxylic acid methyl ester

: 182363-79-7
Methanesulfonic acid 1-cyanomethyl-2,6-dimethoxy-cyclohexa-2,5-dienylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / LiBH₄ / toluene / Heating

2: 100 percent / Et₃N / CH₂Cl₂

With lithium borohydride; triethylamine; In dichloromethane; toluene;
DOI:10.1016/0040-4039(96)01246-4