7-(benzyloxy)-N-(4-fluorophenyl)-8-imino-7,8-dihydropyrimido[5,4-d]pyrimidin-4-amine

Base Information

• Chemical Name: 7-(benzyloxy)-N-(4-fluorophenyl)-8-imino-7,8-dihydropyrimido[5,4-d]pyrimidin-4-amine
• CAS No.: 1196086-74-4
• Molecular Formula: C₁₉H₁₅FN₆O
• Molecular Weight: 362.366

Synonyms:7-(benzyloxy)-N-(4-fluorophenyl)-8-imino-7,8-dihydropyrimido[5,4-d]pyrimidin-4-amine

Chemical Property of 7-(benzyloxy)-N-(4-fluorophenyl)-8-imino-7,8-dihydropyrimido[5,4-d]pyrimidin-4-amine

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Technology Process of 7-(benzyloxy)-N-(4-fluorophenyl)-8-imino-7,8-dihydropyrimido[5,4-d]pyrimidin-4-amine

There total 1 articles about 7-(benzyloxy)-N-(4-fluorophenyl)-8-imino-7,8-dihydropyrimido[5,4-d]pyrimidin-4-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

N-benzyloxyamine (622-33-3) + 9-(4-fluoro-phenyl)-9H-purine-6-carbonitrile → 7-(benzyloxy)-N-(4-fluorophenyl)-8-imino-7,8-dihydropyrimido[5,4-d]pyrimidin-4-amine (1196086-74-4)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 20 ℃; for 22h;

DOI:10.1002/ejoc.200900216

Reference yield: 100.0%

7-(benzyloxy)-N-(4-fluorophenyl)-8-imino-7,8-dihydropyrimido[5,4-d]pyrimidin-4-amine (1196086-74-4) → 8-[(4-fluorophenyl)amino]pyrimido[5,4-d]pyrimidin-4(3H)-one O-benzyloxime (1196086-85-7)

Guidance literature:

With sulfuric acid; In ethanol; water; at 20 ℃; for 0.583333h; chemospecific reaction; Reflux;

DOI:10.1002/ejoc.200900216

Reference yield: 77.0%

7-(benzyloxy)-N-(4-fluorophenyl)-8-imino-7,8-dihydropyrimido[5,4-d]pyrimidin-4-amine (1196086-74-4) → C19H15FN6O*ClH (1196086-84-6)

Guidance literature:

With hydrogenchloride; at 0 ℃; for 0.25h;

DOI:10.1002/ejoc.200900216

upstream raw materials:

N-benzyloxyamine

Downstream raw materials:

8-[(4-fluorophenyl)amino]pyrimido[5,4-d]pyrimidin-4(3H)-one O-benzyloxime

C₁₉H₁₅FN₆O*ClH

7-(benzyloxy)-N-(4-fluorophenyl)-8-imino-7,8-dihydropyrimido[5,4-d]pyrimidin-4-amine dihydrogen sulfate

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