Technology Process of C26H43NO6Si2
There total 3 articles about C26H43NO6Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-chloro-succinimide; potassium hydrogencarbonate;
In
ethyl acetate;
at 20 - 48 ℃;
for 84h;
Inert atmosphere;
DOI:10.1021/ol302691j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: (R,R)-(-)-2,6-bis[2-(hydroxyldiphenylmethyl)-1-pyrrolidinyl-methyl]-4-methylphenole; dimethyl zinc(II) / toluene / 36 h / 20 °C / Inert atmosphere
2: 1H-imidazole / N,N-dimethyl-formamide / 4 h / 0 °C / Inert atmosphere
3: potassium hydrogencarbonate; N-chloro-succinimide / ethyl acetate / 84 h / 20 - 48 °C / Inert atmosphere
With
1H-imidazole; N-chloro-succinimide; (R,R)-(-)-2,6-bis[2-(hydroxyldiphenylmethyl)-1-pyrrolidinyl-methyl]-4-methylphenole; dimethyl zinc(II); potassium hydrogencarbonate;
In
ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol302691j
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1H-imidazole / N,N-dimethyl-formamide / 4 h / 0 °C / Inert atmosphere
2: potassium hydrogencarbonate; N-chloro-succinimide / ethyl acetate / 84 h / 20 - 48 °C / Inert atmosphere
With
1H-imidazole; N-chloro-succinimide; potassium hydrogencarbonate;
In
ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ol302691j