R-(+) estere benzilico dell'acido γ-butirrolatton-γ-3-propionico

Base Information

Chemical Name:R-(+) estere benzilico dell'acido γ-butirrolatton-γ-3-propionico
CAS No.:99393-14-3
Molecular Formula:C₁₄H₁₆O₄
Molecular Weight:248.279
Hs Code.:

Synonyms:R-(+) estere benzilico dell'acido γ-butirrolatton-γ-3-propionico

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of R-(+) estere benzilico dell'acido γ-butirrolatton-γ-3-propionico

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Technology Process of R-(+) estere benzilico dell'acido γ-butirrolatton-γ-3-propionico

There total 9 articles about R-(+) estere benzilico dell'acido γ-butirrolatton-γ-3-propionico which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 122950-95-2
Dibenzyl γ-hydroxypimelate

: 99393-13-2
S-(-) estere benzilico dell'acido γ-butirrolatton-γ-3-propionico

: 99393-14-3
R-(+) estere benzilico dell'acido γ-butirrolatton-γ-3-propionico

Guidance literature:: With pig pancreatic lipase; In diethyl ether; at 30 ℃; for 24h; Title compound not separated from byproducts;
DOI:10.1016/S0957-4166(00)00444-4

Reference yield:

: 502-50-1
4-Ketopimelic acid

: 99393-14-3
R-(+) estere benzilico dell'acido γ-butirrolatton-γ-3-propionico

Guidance literature:: Multi-step reaction with 3 steps

1.1: aq. Cs₂CO₃ / methanol / pH 7.0

1.2: 84 percent / dimethylformamide / 17 h / 20 °C

2.1: 95 percent / sodium borohydride / diethyl ether; methanol / 2 h / -20 °C

3.1: 74 percent / pig pancreatic lipase / diethyl ether / 24 h / 30 °C

With sodium tetrahydroborate; pig pancreatic lipase; caesium carbonate; In methanol; diethyl ether;
DOI:10.1016/S0957-4166(00)00444-4

Reference yield:

: 70957-27-6
Dibenzyl γ-oxopimelate

: 99393-14-3
R-(+) estere benzilico dell'acido γ-butirrolatton-γ-3-propionico

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / sodium borohydride / diethyl ether; methanol / 2 h / -20 °C

2: 74 percent / pig pancreatic lipase / diethyl ether / 24 h / 30 °C

With sodium tetrahydroborate; pig pancreatic lipase; In methanol; diethyl ether;
DOI:10.1016/S0957-4166(00)00444-4