methyl (R)-[2,3,4-⁽³⁾H]-4-(2-(1-(4-chloro-N-(2,5-difluorophenyl)phenylsulfonamido)ethyl)-5-fluorophenyl)butanoate

Base Information

• Chemical Name: methyl (R)-[2,3,4-⁽³⁾H]-4-(2-(1-(4-chloro-N-(2,5-difluorophenyl)phenylsulfonamido)ethyl)-5-fluorophenyl)butanoate
• CAS No.: 1240497-62-4
• Molecular Formula: C₂₅H₂₃ClF₃NO₄S
• Molecular Weight: 531.952

Synonyms:methyl (R)-[2,3,4-⁽³⁾H]-4-(2-(1-(4-chloro-N-(2,5-difluorophenyl)phenylsulfonamido)ethyl)-5-fluorophenyl)butanoate

Chemical Property of methyl (R)-[2,3,4-⁽³⁾H]-4-(2-(1-(4-chloro-N-(2,5-difluorophenyl)phenylsulfonamido)ethyl)-5-fluorophenyl)butanoate

Chemical Property:

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Technology Process of methyl (R)-[2,3,4-⁽³⁾H]-4-(2-(1-(4-chloro-N-(2,5-difluorophenyl)phenylsulfonamido)ethyl)-5-fluorophenyl)butanoate

There total 1 articles about methyl (R)-[2,3,4-⁽³⁾H]-4-(2-(1-(4-chloro-N-(2,5-difluorophenyl)phenylsulfonamido)ethyl)-5-fluorophenyl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl (R,E)-4-(2-(1-(4-chloro-N-(2,5-difluorophenyl)phenylsulfonamido)ethyl)-5-fluorophenyl)but-2-enoate (1240422-97-2) → methyl (R)-[2,3,4-(3)H]-4-(2-(1-(4-chloro-N-(2,5-difluorophenyl)phenylsulfonamido)ethyl)-5-fluorophenyl)butanoate (1240497-62-4)

Guidance literature:

With Wilkinson's catalyst; tritium; In N,N-dimethyl-formamide; toluene; at 21 ℃; for 17h; under 1249.62 Torr;

DOI:10.1002/jlcr.1719

Reference yield:

methyl (R)-[2,3,4-(3)H]-4-(2-(1-(4-chloro-N-(2,5-difluorophenyl)phenylsulfonamido)ethyl)-5-fluorophenyl)butanoate (1240497-62-4) → (R)-[2,3,4-(3)H]-4-(2-(1-(4-chloro-N-(2,5-difluorophenyl)phenylsulfonamido)ethyl)-5-fluorophenyl)butanoic acid (1240497-61-3)

Guidance literature:

methyl (R)-[2,3,4-⁽³⁾H]-4-(2-(1-(4-chloro-N-(2,5-difluorophenyl)phenylsulfonamido)ethyl)-5-fluorophenyl)butanoate; With lithium hydroxide; In water; acetonitrile; at 21 ℃;

With hydrogenchloride; water; In acetonitrile;

DOI:10.1002/jlcr.1719

upstream raw materials:

methyl (R,E)-4-(2-(1-(4-chloro-N-(2,5-difluorophenyl)phenylsulfonamido)ethyl)-5-fluorophenyl)but-2-enoate

Downstream raw materials:

(R)-[2,3,4-⁽³⁾H]-4-(2-(1-(4-chloro-N-(2,5-difluorophenyl)phenylsulfonamido)ethyl)-5-fluorophenyl)butanoic acid

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