C₅₂H₅₆N₈O₇S₄

Base Information

Chemical Name:C₅₂H₅₆N₈O₇S₄
CAS No.:1447195-39-2
Molecular Formula:C₅₂H₅₆N₈O₇S₄
Molecular Weight:1033.33
Hs Code.:

C<sub>52</sub>H<sub>56</sub>N<sub>8</sub>O<sub>7</sub>S<sub>4</sub>

Synonyms:C₅₂H₅₆N₈O₇S₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₂H₅₆N₈O₇S₄

Chemical Property:

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Technology Process of C₅₂H₅₆N₈O₇S₄

There total 16 articles about C₅₂H₅₆N₈O₇S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: C₂₅H₃₀N₄O₅S₂

: 1447194-80-0
C₂₇H₂₈N₄O₃S₂

: 1447195-39-2
C₅₂H₅₆N₈O₇S₄

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 4.5h;
DOI:10.1002/anie.201302106

Reference yield:

: 1447195-24-5
C₄₂H₃₈N₄O₅S₂

: 1447195-39-2
C₅₂H₅₆N₈O₇S₄

Guidance literature:: Multi-step reaction with 2 steps

1: diethylamine / d₇-N,N-dimethylformamide / 0.5 h / 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 4.5 h / 0 - 20 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; In dichloromethane; d₇-N,N-dimethylformamide;
DOI:10.1002/anie.201302106

Reference yield:

: 1447194-67-3
benzyl (4S)-4-(N-fmoc)-amino-3-oxopentanoate

: 1447195-39-2
C₅₂H₅₆N₈O₇S₄

Guidance literature:: Multi-step reaction with 6 steps

1: sulfuryl dichloride / dichloromethane / 1 h / 0 - 20 °C

2: ethanol / 40 °C

3: hydrogen; rosenmund catalyst / tetrahydrofuran; ethanol / 30 °C

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 4.5 h / 0 - 20 °C

5: diethylamine / d₇-N,N-dimethylformamide / 0.5 h / 20 °C

6: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 4.5 h / 0 - 20 °C

With sulfuryl dichloride; rosenmund catalyst; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; In tetrahydrofuran; ethanol; dichloromethane; d₇-N,N-dimethylformamide;
DOI:10.1002/anie.201302106