O-(trans-α-<(2-naphthoyl)amino>cinnamoyl)-L-β-phenyllactic acid

Base Information

• Chemical Name: O-(trans-α-<(2-naphthoyl)amino>cinnamoyl)-L-β-phenyllactic acid
• CAS No.: 169698-16-2
• Molecular Formula: C₂₉H₂₃NO₅
• Molecular Weight: 465.505
• Mol file: 169698-16-2.mol

Synonyms:O-(trans-α-<(2-naphthoyl)amino>cinnamoyl)-L-β-phenyllactic acid

Chemical Property of O-(trans-α-<(2-naphthoyl)amino>cinnamoyl)-L-β-phenyllactic acid

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of O-(trans-α-<(2-naphthoyl)amino>cinnamoyl)-L-β-phenyllactic acid

There total 2 articles about O-(trans-α-<(2-naphthoyl)amino>cinnamoyl)-L-β-phenyllactic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzaldehyde (100-52-7) → O-(trans-α-<(2-naphthoyl)amino>cinnamoyl)-L-β-phenyllactic acid (169698-16-2)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium acetate / acetic anhydride / 3 h / Heating

2: sodium tert-butoxide / tetrahydrofuran / 12 h / Ambient temperature

With sodium acetate; sodium t-butanolate; In tetrahydrofuran; acetic anhydride;

DOI:10.1021/ja00301a025

Reference yield:

L-3-phenyllactic acid (20312-36-1) + (Z)-2-(2-naphthyl)-4-benzylideneoxazolin-5-one → O-(trans-α-<(2-naphthoyl)amino>cinnamoyl)-L-β-phenyllactic acid (169698-16-2)

Guidance literature:

With sodium t-butanolate; In tetrahydrofuran; for 12h; Ambient temperature;

DOI:10.1021/ja00301a025

Reference yield:

O-(trans-α-<(2-naphthoyl)amino>cinnamoyl)-L-β-phenyllactic acid (169698-16-2) → L-3-phenyllactic acid (20312-36-1) + trans-α-<(2-naphthoyl)amon>cinnamic acid

Guidance literature:

carboxypeptidase; In water; dimethyl sulfoxide; at 25 ℃; Kinetics; Equilibrium constant; Thermodynamic data; pH 7.5, ionic strength 0.55, kinetic isotope effect, effect of pH;

DOI:10.1021/ja00301a025

upstream raw materials:

L-3-phenyllactic acid

benzaldehyde

Downstream raw materials:

L-3-phenyllactic acid