3-methyl-5-(3-methylbut-2-enylsulfanyl)-1-phenyl-1H-pyrazole-4-carbaldehyde

Base Information

Chemical Name:3-methyl-5-(3-methylbut-2-enylsulfanyl)-1-phenyl-1H-pyrazole-4-carbaldehyde
CAS No.:160348-48-1
Molecular Formula:C₁₆H₁₈N₂OS
Molecular Weight:286.398
Hs Code.:

Synonyms:3-methyl-5-(3-methylbut-2-enylsulfanyl)-1-phenyl-1H-pyrazole-4-carbaldehyde

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Chemical Property of 3-methyl-5-(3-methylbut-2-enylsulfanyl)-1-phenyl-1H-pyrazole-4-carbaldehyde

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Technology Process of 3-methyl-5-(3-methylbut-2-enylsulfanyl)-1-phenyl-1H-pyrazole-4-carbaldehyde

There total 1 articles about 3-methyl-5-(3-methylbut-2-enylsulfanyl)-1-phenyl-1H-pyrazole-4-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 947-95-5
5-chloro-4-formyl-3-methyl-1-phenyl-1H-pyrazole

: 870-63-3
prenyl bromide

: 160348-48-1
3-methyl-5-(3-methylbut-2-enylsulfanyl)-1-phenyl-1H-pyrazole-4-carbaldehyde

Guidance literature:: prenyl bromide; With thiourea; In ethanol; for 1h; Heating;

With sodium hydroxide; In ethanol; for 1h; Heating;

5-chloro-4-formyl-3-methyl-1-phenyl-1H-pyrazole; In ethanol; for 0.5h; Heating;
DOI:10.1016/S0040-4020(01)01153-X

Reference yield: 87.0%

: 89-25-8
edaravone

: 160348-48-1
3-methyl-5-(3-methylbut-2-enylsulfanyl)-1-phenyl-1H-pyrazole-4-carbaldehyde

: (5aR,10bS)-1,5,5,10-Tetramethyl-3,8-diphenyl-5a,6,8,10b-tetrahydro-3H,5H-4-oxa-7-thia-2,3,8,9-tetraaza-dicyclopenta[a,h]naphthalene

Guidance literature:: edaravone; 3-methyl-5-(3-methylbut-2-enylsulfanyl)-1-phenyl-1H-pyrazole-4-carbaldehyde; With ethylenediaminediacetic acid; In acetonitrile; at 20 ℃; for 0.5h;

In acetonitrile; for 36h; Heating;
DOI:10.1016/S0040-4020(01)01153-X

Reference yield: 87.0%

: 4845-49-2
1,3-diphenyl-5-oxo-4,5-dihydro-1H-pyrazole

: 160348-48-1
3-methyl-5-(3-methylbut-2-enylsulfanyl)-1-phenyl-1H-pyrazole-4-carbaldehyde

: (5aR,10bS)-5,5,10-Trimethyl-1,3,8-triphenyl-5a,6,8,10b-tetrahydro-3H,5H-4-oxa-7-thia-2,3,8,9-tetraaza-dicyclopenta[a,h]naphthalene

Guidance literature:: 1,3-diphenyl-5-oxo-4,5-dihydro-1H-pyrazole; 3-methyl-5-(3-methylbut-2-enylsulfanyl)-1-phenyl-1H-pyrazole-4-carbaldehyde; With ethylenediaminediacetic acid; In acetonitrile; at 20 ℃; for 0.5h;

In acetonitrile; for 36h; Heating;
DOI:10.1016/S0040-4020(01)01153-X