C₂₂H₃₆O₃S

Base Information

Chemical Name:C₂₂H₃₆O₃S
CAS No.:1262416-84-1
Molecular Formula:C₂₂H₃₆O₃S
Molecular Weight:380.592
Hs Code.:

C<sub>22</sub>H<sub>36</sub>O<sub>3</sub>S

Synonyms:C₂₂H₃₆O₃S

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Chemical Property of C₂₂H₃₆O₃S

Chemical Property:

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Technology Process of C₂₂H₃₆O₃S

There total 8 articles about C₂₂H₃₆O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1262416-68-1
C₁₉H₃₂O₃S

: 77-76-9
2,2-dimethoxy-propane

: 1262416-84-1
C₂₂H₃₆O₃S

Guidance literature:: With CSA; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/jo1019909

Reference yield:

: C₁₈H₂₆O₂S

: 1262416-84-1
C₂₂H₃₆O₃S

Guidance literature:: Multi-step reaction with 6 steps

1.1: zinc(II) chloride / tetrahydrofuran / 0.5 h / 20 °C

1.2: 1 h / -78 °C / Inert atmosphere

1.3: 20 °C / pH 2

2.1: diethylzinc / 1,2-dimethoxyethane; hexane; dichloromethane / 0.92 h / 0 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere; Cooling

3.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 °C

4.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / -78 °C / Inert atmosphere

4.2: 20 °C / pH 2

5.1: water; mercury(II) trifluoroacetate; mercury(II) oxide / 1,2-dichloro-ethane / 16 h / 20 °C / Inert atmosphere; Darkness

6.1: CSA / dichloromethane / 3 h / 20 °C

With water; diethylzinc; mercury(II) trifluoroacetate; diisobutylaluminium hydride; Dess-Martin periodane; mercury(II) oxide; zinc(II) chloride; In tetrahydrofuran; 1,2-dimethoxyethane; hexane; dichloromethane; 1,2-dichloro-ethane; toluene;
DOI:10.1021/jo1019909

Reference yield:

: 1262416-44-3
C₁₉H₃₀O₂S

: 1262416-84-1
C₂₂H₃₆O₃S

Guidance literature:: Multi-step reaction with 4 steps

1.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 °C

2.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / -78 °C / Inert atmosphere

2.2: 20 °C / pH 2

3.1: water; mercury(II) trifluoroacetate; mercury(II) oxide / 1,2-dichloro-ethane / 16 h / 20 °C / Inert atmosphere; Darkness

4.1: CSA / dichloromethane / 3 h / 20 °C

With water; mercury(II) trifluoroacetate; diisobutylaluminium hydride; Dess-Martin periodane; mercury(II) oxide; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane; toluene;
DOI:10.1021/jo1019909