2-benzyloxycarbonylamino-3-{7-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-1,3,6,8-tetraoxo-3,6,7,8-tetrahydro-1H-benzo[lmn][3,8]phenanthrolin-2-yl}-propionic acid

Base Information

Chemical Name:2-benzyloxycarbonylamino-3-{7-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-1,3,6,8-tetraoxo-3,6,7,8-tetrahydro-1H-benzo[lmn][3,8]phenanthrolin-2-yl}-propionic acid
CAS No.:919790-04-8
Molecular Formula:C₄₃H₃₉N₃O₉Si
Molecular Weight:769.883
Hs Code.:

2-benzyloxycarbonylamino-3-{7-[2-(<i>tert</i>-butyl-diphenyl-silanyloxy)-ethyl]-1,3,6,8-tetraoxo-3,6,7,8-tetrahydro-1<i>H</i>-benzo[<i>lmn</i>][3,8]phenanthrolin-2-yl}-propionic acid

Synonyms:2-benzyloxycarbonylamino-3-{7-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-1,3,6,8-tetraoxo-3,6,7,8-tetrahydro-1H-benzo[lmn][3,8]phenanthrolin-2-yl}-propionic acid

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Chemical Property of 2-benzyloxycarbonylamino-3-{7-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-1,3,6,8-tetraoxo-3,6,7,8-tetrahydro-1H-benzo[lmn][3,8]phenanthrolin-2-yl}-propionic acid

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Technology Process of 2-benzyloxycarbonylamino-3-{7-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-1,3,6,8-tetraoxo-3,6,7,8-tetrahydro-1H-benzo[lmn][3,8]phenanthrolin-2-yl}-propionic acid

There total 5 articles about 2-benzyloxycarbonylamino-3-{7-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-1,3,6,8-tetraoxo-3,6,7,8-tetrahydro-1H-benzo[lmn][3,8]phenanthrolin-2-yl}-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-2-Benzyloxycarbonylamino-3-(1,3,6,8-tetraoxo-1,3,6,8-tetrahydro-2-oxa-7-aza-pyren-7-yl)-propionic acid

: 91578-89-1
2-((tert-butyldiphenylsilyl)oxy)ethanamine

: 919790-04-8
2-benzyloxycarbonylamino-3-{7-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-1,3,6,8-tetraoxo-3,6,7,8-tetrahydro-1H-benzo[lmn][3,8]phenanthrolin-2-yl}-propionic acid

Guidance literature:: In N,N-dimethyl-formamide; at 110 ℃; for 1.5h;
DOI:10.1021/ja066886+

Reference yield:

: 35761-26-3
(S)-3-amino-2-(((benzyloxy)carbonyl)amino)propanoic acid

: 919790-04-8
2-benzyloxycarbonylamino-3-{7-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-1,3,6,8-tetraoxo-3,6,7,8-tetrahydro-1H-benzo[lmn][3,8]phenanthrolin-2-yl}-propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaOH / H₂O

1.2: H₃PO₄ / 110 °C / pH 5 - 7

2.1: dimethylformamide / 110 °C

With sodium hydroxide; In water; N,N-dimethyl-formamide;
DOI:10.1039/b702255g

Reference yield:

: 81-30-1
1,4,5,8-naphthalenetetracarboxylic dianhydride

: 919790-04-8
2-benzyloxycarbonylamino-3-{7-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-1,3,6,8-tetraoxo-3,6,7,8-tetrahydro-1H-benzo[lmn][3,8]phenanthrolin-2-yl}-propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.95 g / dimethylformamide / 1.5 h / 110 °C

In N,N-dimethyl-formamide;
DOI:10.1021/ja066886+