N-2-(3,4-dimethoxyphenyl)ethyl-1-phenyl-(2-phenylsulfanyl)ethylformamide

Base Information

Chemical Name:N-2-(3,4-dimethoxyphenyl)ethyl-1-phenyl-(2-phenylsulfanyl)ethylformamide
CAS No.:371156-88-6
Molecular Formula:C₂₅H₂₇NO₃S
Molecular Weight:421.56
Hs Code.:

Synonyms:N-2-(3,4-dimethoxyphenyl)ethyl-1-phenyl-(2-phenylsulfanyl)ethylformamide

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Chemical Property of N-2-(3,4-dimethoxyphenyl)ethyl-1-phenyl-(2-phenylsulfanyl)ethylformamide

Chemical Property:

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Technology Process of N-2-(3,4-dimethoxyphenyl)ethyl-1-phenyl-(2-phenylsulfanyl)ethylformamide

There total 4 articles about N-2-(3,4-dimethoxyphenyl)ethyl-1-phenyl-(2-phenylsulfanyl)ethylformamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 2258-42-6
formyl acetic anhydride

: 371156-84-2
N-2-(3,4-dimethoxyphenyl)ethyl-1-phenyl-(2-phenylsulfanyl)ethylamine

: 371156-88-6
N-2-(3,4-dimethoxyphenyl)ethyl-1-phenyl-(2-phenylsulfanyl)ethylformamide

Guidance literature:: With formic acid; at 60 ℃; for 1h;
DOI:10.1248/cpb.49.979

Reference yield:

: 16222-10-9
1-phenyl-2-(phenylthio)ethanone

: 371156-88-6
N-2-(3,4-dimethoxyphenyl)ethyl-1-phenyl-(2-phenylsulfanyl)ethylformamide

Guidance literature:: Multi-step reaction with 3 steps

1: Ti(O-iPr)4 / 3 h / 80 °C

2: NaBH₄ / methanol / 1 h / 20 °C

3: 99 percent / formic acid / 1 h / 60 °C

With titanium(IV) isopropylate; sodium tetrahydroborate; formic acid; In methanol;
DOI:10.1248/cpb.49.979

Reference yield:

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 371156-88-6
N-2-(3,4-dimethoxyphenyl)ethyl-1-phenyl-(2-phenylsulfanyl)ethylformamide

Guidance literature:: Multi-step reaction with 3 steps

1: Ti(O-iPr)4 / 3 h / 80 °C

2: NaBH₄ / methanol / 1 h / 20 °C

3: 99 percent / formic acid / 1 h / 60 °C

With titanium(IV) isopropylate; sodium tetrahydroborate; formic acid; In methanol;
DOI:10.1248/cpb.49.979