2,2,3-trimethyl-6-oxocylohexanecarboxylic acid ethyl ester

Base Information

Chemical Name:2,2,3-trimethyl-6-oxocylohexanecarboxylic acid ethyl ester
CAS No.:408309-84-2
Molecular Formula:C₁₂H₂₀O₃
Molecular Weight:212.289
Hs Code.:

Synonyms:2,2,3-trimethyl-6-oxocylohexanecarboxylic acid ethyl ester

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Chemical Property of 2,2,3-trimethyl-6-oxocylohexanecarboxylic acid ethyl ester

Chemical Property:

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Technology Process of 2,2,3-trimethyl-6-oxocylohexanecarboxylic acid ethyl ester

There total 1 articles about 2,2,3-trimethyl-6-oxocylohexanecarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 408309-84-2
2,2,3-trimethyl-6-oxocylohexanecarboxylic acid ethyl ester

Guidance literature:: With pyridine; methanol; Lindlar's catalyst; Hydrogenation;
DOI:10.1002/hlca.19520350726

Reference yield:

: 408309-84-2
2,2,3-trimethyl-6-oxocylohexanecarboxylic acid ethyl ester

: 79-68-5,35124-16-4,57129-08-5,72244-00-9,73365-47-6,82890-08-2,82890-09-3,89888-04-0,90242-86-7,101325-32-0,117894-47-0,127128-56-7,129314-22-3
(+/-)-trans-γ-irone

Guidance literature:: Multi-step reaction with 4 steps

1.1: BuLi / hexane; tetrahydrofuran / -78 - 20 °C

1.2: tetrahydrofuran; hexane / 2 h / Heating

2.1: 13.4 g / LiAlH₄ / tetrahydrofuran / 0 °C

3.1: DMSO; Et₃N; (COCl)2 / CH₂Cl₂ / -78 - 20 °C

4.1: 9.19 g / toluene / 8 h / Heating

With lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1002/1522-2675(20011219)84:12<3650::AID-HLCA3650>3.0.CO;2-5

Reference yield:

: 408309-84-2
2,2,3-trimethyl-6-oxocylohexanecarboxylic acid ethyl ester

: 1779-49-3
Methyltriphenylphosphonium bromide

: 101170-42-7
2,2,3-trimethyl-6-methylene-cyclohexanecarboxylic acid ethyl ester

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃;

2,2,3-trimethyl-6-oxocylohexanecarboxylic acid ethyl ester; In tetrahydrofuran; hexane; for 2h; Heating;
DOI:10.1002/1522-2675(20011219)84:12<3650::AID-HLCA3650>3.0.CO;2-5