2,2'-<(1,4-phenylene)bis<5,2-(1H-1,2,4-triazolediyl)thio>>bisacetic acid

Base Information

Chemical Name:2,2'-<(1,4-phenylene)bis<5,2-(1H-1,2,4-triazolediyl)thio>>bisacetic acid
CAS No.:160847-54-1
Molecular Formula:C₁₄H₁₂N₆O₄S₂
Molecular Weight:392.419
Hs Code.:

Synonyms:2,2'-<(1,4-phenylene)bis<5,2-(1H-1,2,4-triazolediyl)thio>>bisacetic acid

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Chemical Property of 2,2'-<(1,4-phenylene)bis<5,2-(1H-1,2,4-triazolediyl)thio>>bisacetic acid

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Technology Process of 2,2'-<(1,4-phenylene)bis<5,2-(1H-1,2,4-triazolediyl)thio>>bisacetic acid

There total 4 articles about 2,2'-<(1,4-phenylene)bis<5,2-(1H-1,2,4-triazolediyl)thio>>bisacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 7271-31-0
5,5'-(1,4-phenylene)bis(2,4-dihydro-3H-1,2,4-triazole-3-thione)

: 79-11-8
chloroacetic acid

: 160847-54-1
2,2'-<(1,4-phenylene)bis<5,2-(1H-1,2,4-triazolediyl)thio>>bisacetic acid

Guidance literature:: With sodium hydroxide; In water; for 3h; Reflux;
DOI:10.1080/15421400802697160

Reference yield: 65.0%

: 160847-63-2
diethyl 2,2'-<(1,4-phenylene)bis<5,2-(1H-1,2,4-triazolediyl)thio>>bisacetate

: 160847-54-1
2,2'-<(1,4-phenylene)bis<5,2-(1H-1,2,4-triazolediyl)thio>>bisacetic acid

Guidance literature:: With potassium hydroxide; In methanol; for 24h;

Reference yield:

: 65613-01-6
benzene-1,4-dicarboxylic acid bis<2-(aminothioxomethyl)hydrazide>

: 160847-54-1
2,2'-<(1,4-phenylene)bis<5,2-(1H-1,2,4-triazolediyl)thio>>bisacetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / 10percent aq. NaOH / 3 h / Heating

2: 68 percent / K₂CO₃ / dimethylformamide / 24 h

3: 65 percent / KOH / methanol / 24 h

With potassium hydroxide; sodium hydroxide; potassium carbonate; In methanol; N,N-dimethyl-formamide;