(+)-(3S)-4-hydroxy-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}butanamide

Base Information

Chemical Name:(+)-(3S)-4-hydroxy-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}butanamide
CAS No.:467457-28-9
Molecular Formula:C₃₂H₄₄N₄O₈S₃
Molecular Weight:708.921
Hs Code.:

(+)-(3S)-4-hydroxy-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}butanamide

Synonyms:(+)-(3S)-4-hydroxy-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}butanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(3S)-4-hydroxy-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}butanamide

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Technology Process of (+)-(3S)-4-hydroxy-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}butanamide

There total 2 articles about (+)-(3S)-4-hydroxy-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 91652-58-3
N-(3-aminopropyl)-4-methyl-N-(4-{[(4-methylphenyl)sulfonyl]amino}butyl)benzenesulfonamide

: 147228-21-5
(S)-4-<(tolylsulfonyl)amino>-γ-butyrolactone

: 467457-28-9
(+)-(3S)-4-hydroxy-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}butanamide

Guidance literature:: copper diacetate; In isopropyl alcohol; for 96h;
DOI:10.1002/1522-2675(200206)85:6<1742::AID-HLCA1742>3.0.CO;2-E

Reference yield:

: 96624-91-8
N-<4-butyl>toluol-4-sulfonamid

: 467457-28-9
(+)-(3S)-4-hydroxy-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}butanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / NaBH₄; CF₃COOH / tetrahydrofuran / 2 h / 20 °C

2: 71 percent / Cu(OAc)2 / propan-2-ol / 96 h

With sodium tetrahydroborate; trifluoroacetic acid; copper diacetate; In tetrahydrofuran; isopropyl alcohol;
DOI:10.1002/1522-2675(200206)85:6<1742::AID-HLCA1742>3.0.CO;2-E

Reference yield: 48.0%

: 5469-66-9
propane-1,3-diol ditosylate

: 467457-28-9
(+)-(3S)-4-hydroxy-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}butanamide

: (+)-(8S)-8-(hydroxymethyl)-1,9,13-tris[(4-methylphenyl)sulfonyl]-1,5,9,13-tetraazacycloheptadecan-6-one

Guidance literature:: With caesium carbonate; In dimethyl sulfoxide; at 20 ℃; for 24h;
DOI:10.1002/1522-2675(200206)85:6<1742::AID-HLCA1742>3.0.CO;2-E