succinic acid 5-(2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester 2-[ethyl-(4-phenylazo-phenyl)-amino]-ethyl ester

Base Information

Chemical Name:succinic acid 5-(2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester 2-[ethyl-(4-phenylazo-phenyl)-amino]-ethyl ester
CAS No.:764661-96-3
Molecular Formula:C₃₂H₄₁N₃O₉
Molecular Weight:611.692
Hs Code.:

succinic acid 5-(2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-<i>d</i>][1,3]dioxol-6-yl ester 2-[ethyl-(4-phenylazo-phenyl)-amino]-ethyl ester

Synonyms:succinic acid 5-(2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester 2-[ethyl-(4-phenylazo-phenyl)-amino]-ethyl ester

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Chemical Property of succinic acid 5-(2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester 2-[ethyl-(4-phenylazo-phenyl)-amino]-ethyl ester

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Technology Process of succinic acid 5-(2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester 2-[ethyl-(4-phenylazo-phenyl)-amino]-ethyl ester

There total 2 articles about succinic acid 5-(2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester 2-[ethyl-(4-phenylazo-phenyl)-amino]-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 119613-81-9
3-O-(3-carboxypropanoyl)-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

: 3009-45-8
4'-<2-((hydroxy)ethyl)ethylamino>azobenzene

: 764661-96-3
succinic acid 5-(2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester 2-[ethyl-(4-phenylazo-phenyl)-amino]-ethyl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; at 20 ℃; for 20h;
DOI:10.1002/ejoc.200600686

Reference yield:

: 582-52-5
1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

: 764661-96-3
succinic acid 5-(2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester 2-[ethyl-(4-phenylazo-phenyl)-amino]-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88.6 percent / 4-dimethylaminopyridine; Et₃N / toluene / 2.5 h / Heating

2: 90 percent / N'-(3-dimethylaminopropyl)-N-ethylcarbodiimide hydrochloride; 4-dimethylaminopyridine / tetrahydrofuran / 20 h / 20 °C

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; toluene;
DOI:10.1002/ejoc.200600686