1-[N-Methyl-(t-butoxycarbonylamino)acetamido]-2-(2-fluorobenzoyl)-pyrrole

Base Information

Chemical Name:1-[N-Methyl-(t-butoxycarbonylamino)acetamido]-2-(2-fluorobenzoyl)-pyrrole
CAS No.:97219-51-7
Molecular Formula:C₁₉H₂₂FN₃O₄
Molecular Weight:375.4
Hs Code.:

Synonyms:1-[N-Methyl-(t-butoxycarbonylamino)acetamido]-2-(2-fluorobenzoyl)-pyrrole

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Chemical Property of 1-[N-Methyl-(t-butoxycarbonylamino)acetamido]-2-(2-fluorobenzoyl)-pyrrole

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Technology Process of 1-[N-Methyl-(t-butoxycarbonylamino)acetamido]-2-(2-fluorobenzoyl)-pyrrole

There total 6 articles about 1-[N-Methyl-(t-butoxycarbonylamino)acetamido]-2-(2-fluorobenzoyl)-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 4530-20-5
BOC-glycine

: 117460-73-8
(2-Fluoro-phenyl)-(1-methylamino-1H-pyrrol-2-yl)-methanone

: 97219-51-7
1-[N-Methyl-(t-butoxycarbonylamino)acetamido]-2-(2-fluorobenzoyl)-pyrrole

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; for 5h; Ambient temperature;

Reference yield:

: 97219-46-0
[2-(2-fluorobenzoyl)-1H-pyrrol-1-yl]-carbamic acid,ethyl ester

: 97219-51-7
1-[N-Methyl-(t-butoxycarbonylamino)acetamido]-2-(2-fluorobenzoyl)-pyrrole

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / dimethylformamide / 8 h / Ambient temperature

2: 75 percent / NaOH / ethanol; H₂O / 18 h / Heating

3: 56 percent / dicyclohexylcarbodiimide / CH₂Cl₂ / 5 h / Ambient temperature

With sodium hydroxide; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 97219-47-1
<2-(2-fluorobenzoyl)-1H-pyrrol-1-yl>methylcarbamic acid ethyl ester

: 97219-51-7
1-[N-Methyl-(t-butoxycarbonylamino)acetamido]-2-(2-fluorobenzoyl)-pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / NaOH / ethanol; H₂O / 18 h / Heating

2: 56 percent / dicyclohexylcarbodiimide / CH₂Cl₂ / 5 h / Ambient temperature

With sodium hydroxide; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; water;