(Z)-2-(3,4-dimethoxybenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl stearate

Base Information

Chemical Name:(Z)-2-(3,4-dimethoxybenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl stearate
CAS No.:1311271-95-0
Molecular Formula:C₃₅H₄₈O₆
Molecular Weight:564.763
Hs Code.:

Synonyms:(Z)-2-(3,4-dimethoxybenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl stearate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-(3,4-dimethoxybenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl stearate

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Technology Process of (Z)-2-(3,4-dimethoxybenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl stearate

There total 6 articles about (Z)-2-(3,4-dimethoxybenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl stearate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.3%

: 1311272-24-8
(Z)-2-(3,4-dimethoxybenzylidene)-5-hydroxybenzo[b]furan-3-one

: 112-76-5
Stearoyl chloride

: 1311271-95-0
(Z)-2-(3,4-dimethoxybenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl stearate

Guidance literature:: With pyridine; In dichloromethane; Reflux;
DOI:10.1016/j.bmc.2011.03.063

Reference yield:

: 1311272-35-1
2'-hydroxy-5'-(methoxymethoxy)-3,4-dimethoxychalcone

: 1311271-95-0
(Z)-2-(3,4-dimethoxybenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl stearate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; mercury(II) diacetate / 1 h / 110 °C

2: hydrogenchloride; water / methanol / 0.5 h / Reflux

3: pyridine / dichloromethane / Reflux

With pyridine; hydrogenchloride; mercury(II) diacetate; water; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2011.03.063

Reference yield:

: 1311272-28-2
(Z)-2-(3,4-dimethoxybenzylidene)-5-(methoxymethoxy)benzo[b]furan-3-one

: 1311271-95-0
(Z)-2-(3,4-dimethoxybenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl stearate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; water / methanol / 0.5 h / Reflux

2: pyridine / dichloromethane / Reflux

With pyridine; hydrogenchloride; water; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2011.03.063