Technology Process of C29H24O4
There total 5 articles about C29H24O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: diethyl L-tartrate; titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane / 3 h / -20 °C / Molecular sieve
2.1: sodium hydride / tetrahydrofuran / 1.5 h / 20 °C
2.2: 14 h / Reflux
3.1: p-toluenesulfonyl chloride; pyridine / 48 h / 0 - 20 °C
3.2: 20 °C
4.1: 1,1,1,3',3',3'-hexafluoro-propanol / Sealed tube; Heating
5.1: Dess-Martin periodane / dichloromethane; water / 0 - 20 °C
With
pyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl L-tartrate; 1,1,1,3',3',3'-hexafluoro-propanol; sodium hydride; Dess-Martin periodane; p-toluenesulfonyl chloride;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tet.2014.03.052
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: p-toluenesulfonyl chloride; pyridine / 48 h / 0 - 20 °C
1.2: 20 °C
2.1: 1,1,1,3',3',3'-hexafluoro-propanol / Sealed tube; Heating
3.1: Dess-Martin periodane / dichloromethane; water / 0 - 20 °C
With
pyridine; 1,1,1,3',3',3'-hexafluoro-propanol; Dess-Martin periodane; p-toluenesulfonyl chloride;
In
dichloromethane; water;
DOI:10.1016/j.tet.2014.03.052