2-[2-(furan-2-yl-triethylsilanyloxy-methyl)-phenyl]-1-methyl-1H-imidazole

Base Information

• Chemical Name: 2-[2-(furan-2-yl-triethylsilanyloxy-methyl)-phenyl]-1-methyl-1H-imidazole
• CAS No.: 955044-69-6
• Molecular Formula: C₂₁H₂₈N₂O₂Si
• Molecular Weight: 368.551
• Mol file: 955044-69-6.mol

Synonyms:2-[2-(furan-2-yl-triethylsilanyloxy-methyl)-phenyl]-1-methyl-1H-imidazole

Chemical Property of 2-[2-(furan-2-yl-triethylsilanyloxy-methyl)-phenyl]-1-methyl-1H-imidazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-[2-(furan-2-yl-triethylsilanyloxy-methyl)-phenyl]-1-methyl-1H-imidazole

There total 2 articles about 2-[2-(furan-2-yl-triethylsilanyloxy-methyl)-phenyl]-1-methyl-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

furfural (98-01-1) + triethylsilane (617-86-7) + N-methyl-2-phenyl-1H-imidazole (3475-07-8) → 2-[2-(furan-2-yl-triethylsilanyloxy-methyl)-phenyl]-1-methyl-1H-imidazole (955044-69-6)

Guidance literature:

With MnBr(CO)5; In toluene; at 115 ℃; for 48h;

DOI:10.1002/anie.200702256

Reference yield: 45.0%

(2-furyl)methyl alcohol (98-00-0,25212-86-6,93793-62-5) + triethylsilane (617-86-7) + N-methyl-2-phenyl-1H-imidazole (3475-07-8) → 2-[2-(furan-2-yl-triethylsilanyloxy-methyl)-phenyl]-1-methyl-1H-imidazole (955044-69-6)

Guidance literature:

(2-furyl)methyl alcohol; With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; (E)-3-methylpent-3-en-2-one; potassium carbonate; In toluene; at 150 ℃; for 2h;

triethylsilane; N-methyl-2-phenyl-1H-imidazole; With bromopentacarbonylmanganese(I); In toluene; at 115 ℃; for 24h;

DOI:10.1055/s-0030-1259040

upstream raw materials:

furfural

triethylsilane

N-methyl-2-phenyl-1H-imidazole

(2-furyl)methyl alcohol