2-{2-[2-(4-{2-[2-(2-triisopropylsilanyloxy-ethoxy)-ethoxy]-ethoxy}-phenoxy)-ethoxy]-ethoxy}-ethanol

Base Information

• Chemical Name: 2-{2-[2-(4-{2-[2-(2-triisopropylsilanyloxy-ethoxy)-ethoxy]-ethoxy}-phenoxy)-ethoxy]-ethoxy}-ethanol
• CAS No.: 549529-16-0
• Molecular Formula: C₂₇H₅₀O₈Si
• Molecular Weight: 530.775
• Mol file: 549529-16-0.mol

Synonyms:2-{2-[2-(4-{2-[2-(2-triisopropylsilanyloxy-ethoxy)-ethoxy]-ethoxy}-phenoxy)-ethoxy]-ethoxy}-ethanol

Chemical Property of 2-{2-[2-(4-{2-[2-(2-triisopropylsilanyloxy-ethoxy)-ethoxy]-ethoxy}-phenoxy)-ethoxy]-ethoxy}-ethanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-{2-[2-(4-{2-[2-(2-triisopropylsilanyloxy-ethoxy)-ethoxy]-ethoxy}-phenoxy)-ethoxy]-ethoxy}-ethanol

There total 3 articles about 2-{2-[2-(4-{2-[2-(2-triisopropylsilanyloxy-ethoxy)-ethoxy]-ethoxy}-phenoxy)-ethoxy]-ethoxy}-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

triisopropylsilyl chloride (13154-24-0) + 1,4-bis-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)benzene (134881-72-4) → 2-{2-[2-(4-{2-[2-(2-triisopropylsilanyloxy-ethoxy)-ethoxy]-ethoxy}-phenoxy)-ethoxy]-ethoxy}-ethanol (549529-16-0)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(03)00242-9

Reference yield:

2-[2-(chloroethoxy)ethoxy]ethanol (5197-62-6) → 2-{2-[2-(4-{2-[2-(2-triisopropylsilanyloxy-ethoxy)-ethoxy]-ethoxy}-phenoxy)-ethoxy]-ethoxy}-ethanol (549529-16-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / t-BuOK / 2-methyl-propan-2-ol / 92 h / Heating

2: 46 percent / imidazole / dimethylformamide

With 1H-imidazole; potassium tert-butylate; In N,N-dimethyl-formamide; tert-butyl alcohol;

DOI:10.1016/S0040-4039(03)00242-9

Reference yield:

hydroquinone (123-31-9,8027-02-9) → 2-{2-[2-(4-{2-[2-(2-triisopropylsilanyloxy-ethoxy)-ethoxy]-ethoxy}-phenoxy)-ethoxy]-ethoxy}-ethanol (549529-16-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / t-BuOK / 2-methyl-propan-2-ol / 92 h / Heating

2: 46 percent / imidazole / dimethylformamide

With 1H-imidazole; potassium tert-butylate; In N,N-dimethyl-formamide; tert-butyl alcohol;

DOI:10.1016/S0040-4039(03)00242-9

upstream raw materials:

triisopropylsilyl chloride

1,4-bis-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)benzene

2-[2-(chloroethoxy)ethoxy]ethanol

hydroquinone

Downstream raw materials:

Toluene-4-sulfonic acid 2-{2-[2-(4-{2-[2-(2-triisopropylsilanyloxy-ethoxy)-ethoxy]-ethoxy}-phenoxy)-ethoxy]-ethoxy}-ethyl ester

[3-hydroxymethyl-5-methyl-2-(2-{2-[2-(4-{2-[2-(2-triisopropylsilanyloxy-ethoxy)-ethoxy]-ethoxy}-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol

[5-methyl-2-(2-{2-[2-(4-{2-[2-(2-triisopropylsilanyloxy-ethoxy)-ethoxy]-ethoxy}-phenoxy)-ethoxy]-ethoxy}-ethoxy)-3-triisopropylsilanyloxymethyl-phenyl]-methanol