ethyl (4S)-4-acetoxy-4-[(4R)-4-(acetoxymethyl)-3-benzyl-2-oxooxazolidin-4-yl]butanoate

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Chemical Name:ethyl (4S)-4-acetoxy-4-[(4R)-4-(acetoxymethyl)-3-benzyl-2-oxooxazolidin-4-yl]butanoate
CAS No.:1421940-31-9
Molecular Formula:C₂₁H₂₇NO₈
Molecular Weight:421.447
Hs Code.:

Synonyms:ethyl (4S)-4-acetoxy-4-[(4R)-4-(acetoxymethyl)-3-benzyl-2-oxooxazolidin-4-yl]butanoate

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Chemical Property of ethyl (4S)-4-acetoxy-4-[(4R)-4-(acetoxymethyl)-3-benzyl-2-oxooxazolidin-4-yl]butanoate

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Technology Process of ethyl (4S)-4-acetoxy-4-[(4R)-4-(acetoxymethyl)-3-benzyl-2-oxooxazolidin-4-yl]butanoate

There total 7 articles about ethyl (4S)-4-acetoxy-4-[(4R)-4-(acetoxymethyl)-3-benzyl-2-oxooxazolidin-4-yl]butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1421940-30-8
ethyl (4S)-4-[(4R)-3-benzyl-4-(hydroxymethyl)-2-oxooxazolidin-4-yl]-4-hydroxybutanoate

: 108-24-7
acetic anhydride

: 1421940-31-9
ethyl (4S)-4-acetoxy-4-[(4R)-4-(acetoxymethyl)-3-benzyl-2-oxooxazolidin-4-yl]butanoate

Guidance literature:: With pyridine; dmap; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetasy.2012.12.003

Reference yield:

: 1421940-24-0
ethyl (4S,2E)-4-{(4R)-3-benzyl-4-[(1S)-2-(benzyloxy)-1-hydroxyethyl]-2-oxooxazolidin-4-yl}-4-hydroxybut-2-enoate

: 1421940-31-9
ethyl (4S)-4-acetoxy-4-[(4R)-4-(acetoxymethyl)-3-benzyl-2-oxooxazolidin-4-yl]butanoate

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen; 5%-palladium/activated carbon / ethanol / 19 h / 20 °C / Inert atmosphere

2: sodium periodate / methanol; water / 1 h / 20 °C / Inert atmosphere

3: sodium tetrahydroborate / ethanol / 2.17 h / 0 - 20 °C / Inert atmosphere

4: pyridine; dmap / 20 °C / Inert atmosphere

With pyridine; dmap; sodium tetrahydroborate; sodium periodate; 5%-palladium/activated carbon; hydrogen; In methanol; ethanol; water;
DOI:10.1016/j.tetasy.2012.12.003

Reference yield:

: 1430738-72-9
C₂₁H₂₃NO₆

: 1421940-31-9
ethyl (4S)-4-acetoxy-4-[(4R)-4-(acetoxymethyl)-3-benzyl-2-oxooxazolidin-4-yl]butanoate

Guidance literature:: Multi-step reaction with 5 steps

1: benzoic acid / water / 26.5 h / 20 °C / Inert atmosphere

2: hydrogen; 5%-palladium/activated carbon / ethanol / 19 h / 20 °C / Inert atmosphere

3: sodium periodate / methanol; water / 1 h / 20 °C / Inert atmosphere

4: sodium tetrahydroborate / ethanol / 2.17 h / 0 - 20 °C / Inert atmosphere

5: pyridine; dmap / 20 °C / Inert atmosphere

With pyridine; dmap; sodium tetrahydroborate; sodium periodate; 5%-palladium/activated carbon; hydrogen; benzoic acid; In methanol; ethanol; water;
DOI:10.1016/j.tetasy.2012.12.003