(6-Bromo-1,4-dioxa-8-azaspiro[4.5]dec-8-yl)phenylmethanone

Base Information

Chemical Name:(6-Bromo-1,4-dioxa-8-azaspiro[4.5]dec-8-yl)phenylmethanone
CAS No.:84157-06-2
Molecular Formula:C₁₄H₁₆BrNO₃
Molecular Weight:326.19
Hs Code.:
DSSTox Substance ID:DTXSID401192977

Synonyms:(6-Bromo-1,4-dioxa-8-azaspiro[4.5]dec-8-yl)phenylmethanone;DTXSID401192977;84157-06-2

Suppliers and Price of (6-Bromo-1,4-dioxa-8-azaspiro[4.5]dec-8-yl)phenylmethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (6-Bromo-1,4-dioxa-8-azaspiro[4.5]dec-8-yl)phenylmethanone

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:325.03136
Heavy Atom Count:19
Complexity:338

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CN(CC(C12OCCO2)Br)C(=O)C3=CC=CC=C3

Technology Process of (6-Bromo-1,4-dioxa-8-azaspiro[4.5]dec-8-yl)phenylmethanone

There total 3 articles about (6-Bromo-1,4-dioxa-8-azaspiro[4.5]dec-8-yl)phenylmethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.6%

: 84157-05-1
phenyl(1,4-dioxa-8-azaspiro[4.5]decan-8-yl)methanone

: 84157-06-2
N-benzoyl-3-bromo-4-piperidone ethylene ketal

Guidance literature:: With bromine; In ethylene glycol;

Reference yield:

: 98-88-4
benzoyl chloride

: 84157-06-2
N-benzoyl-3-bromo-4-piperidone ethylene ketal

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₃N / diethyl ether / 2 h

2: 92.6 percent / bromine / ethane-1,2-diol

With bromine; triethylamine; In diethyl ether; ethylene glycol;

Reference yield:

: 177-11-7
4,4-ethylenedioxy-piperidine

: 84157-06-2
N-benzoyl-3-bromo-4-piperidone ethylene ketal

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₃N / diethyl ether / 2 h

2: 92.6 percent / bromine / ethane-1,2-diol

With bromine; triethylamine; In diethyl ether; ethylene glycol;