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PChd-L-Pro-OBzl

Base Information Edit
  • Chemical Name:PChd-L-Pro-OBzl
  • CAS No.:74763-79-4
  • Molecular Formula:C32H39NO3
  • Molecular Weight:485.667
  • Hs Code.:
  • Mol file:74763-79-4.mol
PChd-L-Pro-OBzl

Synonyms:PChd-L-Pro-OBzl

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Chemical Property of PChd-L-Pro-OBzl Edit
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Technology Process of PChd-L-Pro-OBzl

There total 12 articles about PChd-L-Pro-OBzl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 2,6-dimethylpyridine; N,N,N,N-tetraethylammonium tetrafluoroborate; In dichloromethane;
Guidance literature:
Multi-step reaction with 7 steps
1: 1.) N-methylmorpholin, 1-hydroxybenzotriazole; 2.) N,N'-dicyclohexylcarbodiimide / 1.) CH2Cl2; 2.) CH2Cl2, 30 min, 0 deg C; 12 h at room temp.
2: 97 percent / 1 N HCl, H2 / Pd/10percent on charcoal / methanol / 4 h
3: 89 percent / 2,6-dimethylpyridine; tetraethylammonium tetrafluoroborate / CH2Cl2 / 8 h / anodic oxidation
4: 60 percent / 1 N NaOH / methanol / 4 h
5: 1.) N-methylmorpholin, 1-hydroxybenzotriazole; 2.) N,N'-dicyclohexylcarbodiimide / 1.) CH2Cl2; 2.) CH2Cl2, 1 h, 0 deg C; 24 h at room temp.
6: 90 percent / 1 N HCl, H2 / Pd/10percent on charcoal / methanol / 4 h
7: 59 percent / 2,6-dimethylpyridine; tetraethylammonium tetrafluoroborate / CH2Cl2 / 8 h / anodic oxidation
With 4-methyl-morpholine; 2,6-dimethylpyridine; hydrogenchloride; sodium hydroxide; hydrogen; N,N,N,N-tetraethylammonium tetrafluoroborate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1002/jlac.198219820608
Guidance literature:
Multi-step reaction with 6 steps
1: 97 percent / 1 N HCl, H2 / Pd/10percent on charcoal / methanol / 4 h
2: 89 percent / 2,6-dimethylpyridine; tetraethylammonium tetrafluoroborate / CH2Cl2 / 8 h / anodic oxidation
3: 60 percent / 1 N NaOH / methanol / 4 h
4: 1.) N-methylmorpholin, 1-hydroxybenzotriazole; 2.) N,N'-dicyclohexylcarbodiimide / 1.) CH2Cl2; 2.) CH2Cl2, 1 h, 0 deg C; 24 h at room temp.
5: 90 percent / 1 N HCl, H2 / Pd/10percent on charcoal / methanol / 4 h
6: 59 percent / 2,6-dimethylpyridine; tetraethylammonium tetrafluoroborate / CH2Cl2 / 8 h / anodic oxidation
With 4-methyl-morpholine; 2,6-dimethylpyridine; hydrogenchloride; sodium hydroxide; hydrogen; N,N,N,N-tetraethylammonium tetrafluoroborate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1002/jlac.198219820608
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