C₂₉H₄₄O₁₁Si

Base Information

Chemical Name:C₂₉H₄₄O₁₁Si
CAS No.:1379535-90-6
Molecular Formula:C₂₉H₄₄O₁₁Si
Molecular Weight:596.747
Hs Code.:

C<sub>29</sub>H<sub>44</sub>O<sub>11</sub>Si

Synonyms:C₂₉H₄₄O₁₁Si

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Chemical Property of C₂₉H₄₄O₁₁Si

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Technology Process of C₂₉H₄₄O₁₁Si

There total 9 articles about C₂₉H₄₄O₁₁Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1379535-88-2
C₃₆H₅₀O₁₁Si

: 1379535-90-6
C₂₉H₄₄O₁₁Si

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; methanol; at 20 ℃; for 8h; Inert atmosphere;
DOI:10.1021/ol301107m

Reference yield:

: 2-bromo-3,6-bis(methoxymethoxy)benzaldehyde

: 1379535-90-6
C₂₉H₄₄O₁₁Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium tetrahydroborate / methanol / 0.33 h / 0 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.17 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: tert.-butyl lithium / diethyl ether; pentane / 0.08 h / -78 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide / 3 h / 20 °C / Inert atmosphere

5.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; methanol / 8 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; tert.-butyl lithium; sodium hydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil; pentane;
DOI:10.1021/ol301107m

Reference yield:

: 1178892-65-3
4-(((tert-butyldimethylsilyl)oxy)methyl)-2,6-bis-(methoxymethoxy)benzaldehyde

: 1379535-90-6
C₂₉H₄₄O₁₁Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: tert.-butyl lithium / diethyl ether; pentane / 0.08 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide / 3 h / 20 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; methanol / 8 h / 20 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; tert.-butyl lithium; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; dimethyl sulfoxide; pentane;
DOI:10.1021/ol301107m