ClC₄H₃NCC₆H₅C₄N(CH₃)2CH₂CH₃

Base Information

Chemical Name:ClC₄H₃NCC₆H₅C₄N(CH₃)2CH₂CH₃
CAS No.:1355953-56-8
Molecular Formula:C₁₉H₁₉ClN₂
Molecular Weight:310.826
Hs Code.:

ClC<sub>4</sub>H<sub>3</sub>NCC<sub>6</sub>H<sub>5</sub>C<sub>4</sub>N(CH<sub>3</sub>)2CH<sub>2</sub>CH<sub>3</sub>

Synonyms:ClC₄H₃NCC₆H₅C₄N(CH₃)2CH₂CH₃

Suppliers and Price of ClC₄H₃NCC₆H₅C₄N(CH₃)2CH₂CH₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ClC₄H₃NCC₆H₅C₄N(CH₃)2CH₂CH₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ClC₄H₃NCC₆H₅C₄N(CH₃)2CH₂CH₃

There total 7 articles about ClC₄H₃NCC₆H₅C₄N(CH₃)2CH₂CH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 517-22-6
2,4-dimethyl-3-ethyl-pyrrole

: 142231-06-9
2-benzoyl-5-chloropyrrole

: 1355953-56-8
ClC₄H₃NCC₆H₅C₄N(CH₃)2CH₂CH₃

Guidance literature:: 5-chloro-2-benzoylpyrrole; With trichlorophosphate; In dichloromethane; at 20 ℃; for 1h;

2,4-dimethyl-3-ethyl-pyrrole; In dichloromethane; for 36h;
DOI:10.1039/c1dt10797f

Reference yield:

: 98-88-4
benzoyl chloride

: 1355953-56-8
ClC₄H₃NCC₆H₅C₄N(CH₃)2CH₂CH₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 4 h / 20 °C / Cooling with ice

2.1: trichlorophosphate / 20 °C / Inert atmosphere

2.2: 24 h / 20 °C / Inert atmosphere

3.1: copper(II) choride dihydrate / acetonitrile / 24 h / Reflux

4.1: trichlorophosphate / dichloromethane / 1 h / 20 °C

4.2: 12 h / 20 °C

With copper(II) choride dihydrate; triethylamine; trichlorophosphate; In dichloromethane; acetonitrile;
DOI:10.1039/d0ob00082e

Reference yield:

: 123-54-6,81235-32-7
acetylacetone

: 1355953-56-8
ClC₄H₃NCC₆H₅C₄N(CH₃)2CH₂CH₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid; sodium nitrite / water / 12 h / 0 - 25 °C

1.2: 1 h / 60 °C / Cooling with ice

2.1: potassium hydroxide / 1,2-dimethoxyethane / 4 h / 160 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / Cooling with ice; Reflux

4.1: trichlorophosphate / dichloromethane / 1 h / 20 °C

4.2: 12 h / 20 °C

With lithium aluminium tetrahydride; acetic acid; potassium hydroxide; sodium nitrite; trichlorophosphate; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1039/d0ob00082e