(R)-(-)-N-[(1E)-(4-chlorophenyl)methylene]-2-methyl-2-propanesulfinamide

Base Information

• Chemical Name: (R)-(-)-N-[(1E)-(4-chlorophenyl)methylene]-2-methyl-2-propanesulfinamide
• CAS No.: 336105-23-8
• Molecular Formula: C₁₁H₁₄ClNOS
• Molecular Weight: 243.757

Synonyms:(R)-(-)-N-[(1E)-(4-chlorophenyl)methylene]-2-methyl-2-propanesulfinamide

Chemical Property of (R)-(-)-N-[(1E)-(4-chlorophenyl)methylene]-2-methyl-2-propanesulfinamide

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Technology Process of (R)-(-)-N-[(1E)-(4-chlorophenyl)methylene]-2-methyl-2-propanesulfinamide

There total 1 articles about (R)-(-)-N-[(1E)-(4-chlorophenyl)methylene]-2-methyl-2-propanesulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-chlorobenzaldehyde (104-88-1) + (R)-2-methylpropane-2-sulfinamide (196929-78-9) → (R)-(-)-N-[(1E)-(4-chlorophenyl)methylene]-2-methyl-2-propanesulfinamide (336105-23-8)

Guidance literature:

With pyridinium p-toluenesulfonate; magnesium sulfate; In dichloromethane; at 20 ℃;

DOI:10.1016/S0957-4166(02)00099-X

Reference yield: 98.0%

allyl bromide (106-95-6) + (R)-(-)-N-[(1E)-(4-chlorophenyl)methylene]-2-methyl-2-propanesulfinamide (336105-23-8) → (RS,1S)-N-(tert-butanesulfinyl)-1-(4-chlorophenyl)but-3-en-1-amine

Guidance literature:

With In(OSO₂CF₃)3; zinc; In tetrahydrofuran; at 20 ℃; for 10h;

DOI:10.1021/ol062216x

Reference yield: 96.0%

allyl bromide (106-95-6) + (R)-(-)-N-[(1E)-(4-chlorophenyl)methylene]-2-methyl-2-propanesulfinamide (336105-23-8) → (R)-N-((R)-1-(4-chlorophenyl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide + (RS,1S)-N-(tert-butanesulfinyl)-1-(4-chlorophenyl)but-3-en-1-amine

Guidance literature:

With water; zinc; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 20 ℃; for 12h;

DOI:10.1021/ol062216x

upstream raw materials:

4-chlorobenzaldehyde

(R)-2-methylpropane-2-sulfinamide

Downstream raw materials:

(R)-(4-chlorophenyl)(phenyl)methylamine

(S)-4-chloro-α-phenyl-benzenemethanamine

(R(S))-N-((R)-1-(4-chlorophenyl)-1-phenylmethyl)-2-methylpropane-2-sulfinamide

(R_S,S)-(1-(4-chlorophenyl)-1-phenylmethyl)-2-methylpropanesulfinamide

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