3-(benzyloxycarbonyl)aminopropyl 2,3-O-isopropylidene-α-D-mannopyranoside 12

Base Information

Chemical Name:3-(benzyloxycarbonyl)aminopropyl 2,3-O-isopropylidene-α-D-mannopyranoside 12
CAS No.:1262208-34-3
Molecular Formula:C₂₀H₂₉NO₈
Molecular Weight:411.452
Hs Code.:

Synonyms:3-(benzyloxycarbonyl)aminopropyl 2,3-O-isopropylidene-α-D-mannopyranoside 12

Suppliers and Price of 3-(benzyloxycarbonyl)aminopropyl 2,3-O-isopropylidene-α-D-mannopyranoside 12

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-(benzyloxycarbonyl)aminopropyl 2,3-O-isopropylidene-α-D-mannopyranoside 12

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-(benzyloxycarbonyl)aminopropyl 2,3-O-isopropylidene-α-D-mannopyranoside 12

There total 5 articles about 3-(benzyloxycarbonyl)aminopropyl 2,3-O-isopropylidene-α-D-mannopyranoside 12 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1236190-06-9
3-(benzyloxycarbonyl)aminopropyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

: 77-76-9
2,2-dimethoxy-propane

: 1262208-34-3
3-(benzyloxycarbonyl)aminopropyl 2,3-O-isopropylidene-α-D-mannopyranoside 12

Guidance literature:: 3-(benzyloxycarbonyl)aminopropyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside; With sodium methylate; In methanol;

2,2-dimethoxy-propane; With toluene-4-sulfonic acid; In acetone; for 1h;

Reference yield:

: C₂₃H₃₃NO₈

: 1262208-34-3
3-(benzyloxycarbonyl)aminopropyl 2,3-O-isopropylidene-α-D-mannopyranoside 12

Guidance literature:: With water; In methanol; at 20 ℃; for 6h; regioselective reaction;
DOI:10.1021/ol1026188

Reference yield:

: 34637-22-4
3-[(N-benzyloxycarbonyl)amino]propanol

: 1262208-34-3
3-(benzyloxycarbonyl)aminopropyl 2,3-O-isopropylidene-α-D-mannopyranoside 12

Guidance literature:: Multi-step reaction with 4 steps

1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / -10 - 20 °C / Inert atmosphere

2.1: sodium methylate / methanol / 12 h / 20 °C

2.2: Dowex H⁺

3.1: toluene-4-sulfonic acid / acetone / 1 h / 20 °C

4.1: water / methanol / 6 h / 20 °C

With trimethylsilyl trifluoromethanesulfonate; water; sodium methylate; toluene-4-sulfonic acid; In methanol; dichloromethane; acetone;
DOI:10.1021/ol1026188